Microwave Assisted One Pot Synthesis of Substituted 3-Formyl Benzoates Using Vilsmeier Reagent

Srinivasan Selvi Organic Chemistry Division, Central Leather Research Institute, Adyar, Chennai, 600 020, INDIA Fax: E-mail: [email protected]

Paramasivan T. Perumal Organic Chemistry Division, Central Leather Research Institute, Adyar, Chennai, 600 020, INDIA Fax: E-mail: [email protected]

Abstract

A facile one pot conversion of alkyl diacylacetates to 2,6-dichloro-3-formyl benzoates using Vilsmeier reagent in a two pronged strategy - conventional heating and microwave irradiation method is reported. The reaction time has been brought down from hours to seconds in microwave irradiation method.

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Microwave Assisted One Pot Synthesis of Substituted 3-Formyl Benzoates Using Vilsmeier Reagent

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Microwave Assisted One Pot Synthesis of Substituted 3-Formyl Benzoates Using Vilsmeier Reagent

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