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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 30, 2000 - Issue 21
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Original Articles

Racemization-Free Recovery of α-Hydroxyphosphonates from Their Carboxylic Esters

Dorota G. Piotrowska Institute of Chemistry, Faculty of Pharmacy, Medical University of Łódź, 90-151 Łédź, Muszyńskiego 1, Poland
,
Anetta Halajewska-Wosik Institute of Chemistry, Faculty of Pharmacy, Medical University of Łódź, 90-151 Łédź, Muszyńskiego 1, Poland
&
Andrzej E. Wróblewski Institute of Chemistry, Faculty of Pharmacy, Medical University of Łódź, 90-151 Łédź, Muszyńskiego 1, Poland
Pages 3935-3940 | Accepted 21 Dec 1999, Published online: 04 Dec 2007
 
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Abstract

Ammonolysis (25% aqueous NH3 - alcohols or THF) of carboxylic esters obtained from diastereoisomerically pure α-hydroxyphosphonates leads to recovery of the phosphonates without racemization in good to excellent yields.

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