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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 30, 2000 - Issue 20
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Original Articles

Stereocontrolled Iodolactonization of Acyclic Olefinic Amides

Hyun-Joon Ha Department of Chemistry, Hankuk University of Foreign Studies Yongin, Kyunggi-Do, 449--791, Korea
,
Sang-Youn Lee Department of Chemistry, Hankuk University of Foreign Studies Yongin, Kyunggi-Do, 449--791, Korea
&
Young-Soo Park Department of Chemistry, Hankuk University of Foreign Studies Yongin, Kyunggi-Do, 449--791, Korea
Pages 3645-3650 | Received 03 Aug 1999, Published online: 04 Dec 2007
 
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Abstract

Acyclic olefinic amides were iodolactonized in the mixed solvent of CH3CN and H2O (90:102 v/v) under reflux to give products with trans configuration of the newly formed iodomethyl to the inherent alkyl group in high yield.

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