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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 30, 2000 - Issue 19
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Original Articles

Selective One-Pot N-Monomethylation of 2-Nitroanilines Under Ptc Conditions

Sergei Voskresensky Institute of Organic Chemistry, Polish Academy of Sciences, Kasprzaka 44/52, PL 01-224, Warsaw, Poland
&
Mieczyslaw Makosza Institute of Organic Chemistry, Polish Academy of Sciences, Kasprzaka 44/52, PL 01-224, Warsaw, Poland
Pages 3523-3526 | Accepted 09 Dec 1999, Published online: 04 Dec 2007
 
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Abstract

Direct PTC methylation of 2-nitroanilines with dimethyl sulfate gave selectively N-monomethylated products. A variety of N-methyl-2-nitroanilines were prepared in this way.

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