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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 30, 2000 - Issue 1
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Original Articles

One-Pot Preparation of Fischer Carbene Complexes by Solid-Liquid Phase Transfer Catalysis

Qi-Huang Zheng Department of Chemistry, The University of Chicago, Searle Chemistry Laboratory, Chicago, IL, 60637, USA; Department of Radiology, Indiana University Medical Center, 975W. Walnut St., IB028, Indianapolis, IN, 46202--5121, USA
&
Jing Su Department of Chemistry, The University of Chicago, Searle Chemistry Laboratory, Chicago, IL, 60637, USA
Pages 177-185 | Received 28 May 1999, Published online: 04 Dec 2007
 
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Abstract

Neutral Fischer carbene complexes bearing alkyloxy groups have been synthesized by direct alkylation of the lithium acylmetalates with alkyl iodides under solid-liquid phase transfer catalysis (PTC).

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