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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 30, 2000 - Issue 16
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Original Articles

TrocCl Mediated Efficient Synthesis of Nitriles from Primary Amides

D. Subhas Bose Organic Chemistry Division III, Fine Chemicals Laboratory, Indian Institute of Chemical Technology, Hyderabad, 500 007, India
&
K. Kiran Kumar Organic Chemistry Division III, Fine Chemicals Laboratory, Indian Institute of Chemical Technology, Hyderabad, 500 007, India
Pages 3047-3052 | Received 07 Sep 1999, Published online: 04 Dec 2007
 
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Abstract

In order to establish a rapid conversion method of primary amides to nitriles, various types of carboxamides were treated with 2,2,2-trichloroethyl chloroformate and Et3N, as a dehydrating agent to obtain the desired nitriles in 82–95% yields.

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