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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 35, 2005 - Issue 17
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Original Articles

Solid‐State Condensation Reactions Between Aldehydes and 5,5‐Dimethyl‐1,3‐cyclohexanedione by Grinding at Room Temperature

Tong‐Shou Jin Department of Chemistry, College of Chemistry and Environmental Science, Hebei University, Baoding, Hebei Province, ChinaCorrespondence[email protected]
,
Jian‐She Zhang Department of Chemistry, College of Chemistry and Environmental Science, Hebei University, Baoding, Hebei Province, China
,
Ai‐Qing Wang Department of Chemistry, College of Chemistry and Environmental Science, Hebei University, Baoding, Hebei Province, China
&
Tong‐Shuang Li Department of Chemistry, College of Chemistry and Environmental Science, Hebei University, Baoding, Hebei Province, China
Pages 2339-2345 | Received 28 Feb 2005, Published online: 18 Aug 2006
 
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Abstract

An efficient and convenient approach to the synthesis of the two different products from aldehydes and 5,5‐dimethyl‐1,3‐cyclohexanedione in the solid state by grinding is described. This method provides several advantages such as environmental friendliness, high yields, and simple workup procedure.

Acknowledgments

This project was supported by the National Natural Science Foundation of China (Nos. 29872011 and 29572039); Educational Ministry of China, Educational Department of Hebei Province (990104); and Science and Technology Commission of Hebei Province.

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