Facile Preparation and Purification of Mono tert‐Butyl Malonate

Vitali I. Tararov Leibniz‐Institut für Organische Katalyse e.V., Rostock, Germany

Andrei Korostylev Leibniz‐Institut für Organische Katalyse e.V., Rostock, Germany

Gerd König Ratiopharm GmbH, Ulm, Germany

Armin Börner Leibniz‐Institut für Organische Katalyse e.V., Rostock, Germany; Institut für Chemie der Universität Rostock, Rostock, GermanyCorrespondence[email protected]

Abstract

Reaction of Meldrum's acid with tert‐BuOH gives tert‐BuO₂CCH₂CO₂H, which can be easily purified via its corresponding crystalline ammonium salt and subsequent acidification.

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Acknowledgment

We thank K. Mevius for skilled technical assistance. Financial support from Ratiopharm GmbH is gratefully acknowledged.

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Facile Preparation and Purification of Mono tert‐Butyl Malonate

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Facile Preparation and Purification of Mono tert‐Butyl Malonate

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