Efficient Method for Silylation of p‐Nitrobenzyl‐2‐diazoacetoacetate

Neera Tewari Chemical Research Division, Ranbaxy Research Laboratories, Gurgaon, Haryana, India

Bishwa Prakash Rai Chemical Research Division, Ranbaxy Research Laboratories, Gurgaon, Haryana, India

Hashim Nizar Chemical Research Division, Ranbaxy Research Laboratories, Gurgaon, Haryana, IndiaCorrespondence[email protected]

Shailendra Kumar Singh Chemical Research Division, Ranbaxy Research Laboratories, Gurgaon, Haryana, India

Abstract

An efficient new method for the silylation of p‐nitrobenzyl‐2‐diazoacetoacetate using hexamethyl disilane and iodine is presented.

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Acknowledgment

We are grateful to the Analytical Division of Ranbaxy Research Laboratories for their analytical support.

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Efficient Method for Silylation of p‐Nitrobenzyl‐2‐diazoacetoacetate

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Efficient Method for Silylation of p‐Nitrobenzyl‐2‐diazoacetoacetate

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