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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 36, 2006 - Issue 2
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Abstracts

Graphical Abstracts

Pages i-vi | Published online: 15 Aug 2006
 

Abstract

Graphical Abstract Section

Abstract

Synth. Commun. 2006, 35, 137

TRIPHENYLPHOSPHINE–IODINE: AN EFFICIENT REAGENT SYSTEM FOR THE SYNTHESIS OF NITRILES FROM ALDOXIMES

A. Venkat Narsaiah, D. Sreenu, and K. Nagaiah

Division of Organic Chemistry, Fine Chemicals Laboratory, Indian Institute of Chemical Technology, Hyderabad 500 007, India

Abstract

Synth. Commun. 2006, 35, 141

REGIOSELECTIVE SYNTHESIS OF NOVEL SPIROOXINDOLO AND SPIROINDANO NITRO PYRROLIDINES THROUGH 3 + 2 CYCLOADDITION REACTION

Mahalingam Poornachandran, Rajendran Muruganantham, and Ragavachary Raghunathan

Department of Organic Chemistry, University of Madras, Guindy Campus, Chennai 600 025, India

Abstract

Synth. Commun. 2006, 35, 151

SYNTHESIS OF NOVEL OXIME FUNCTIONALIZED ALDOL PRODUCTS VIA MICHAEL ADDITION OF OXIMES ONTO BAYLIS–HILLMAN ADDUCTS

Debnath Bhuniya, Srinivas Gujjary, and Sujata Sengupta

Metabolic Disorder (Chemistry) Group, Dr. Reddy's Laboratories Ltd.—Discovery Research, Miyapur, Bollaram Road, Hyderabad 500 049, India

Abstract

Synth. Commun. 2006, 35, 165

DMSO/NaNO2/49% HBr: A NOVEL AND POWERFUL OXIDANT FOR THE DIRECT CONVERSION OF PRIMARY BENZYLAMINES TO BENZOIC ACIDS

Ramesh Naik and M. A. Pasha

Department of Studies in Chemistry, Central College Campus, Bangalore University, Bangalore 560 001, India

A mixture of DMSO, NaNO2, and 49% HBr is found to oxidize primary benzylamines to benzoic acids at 100°C.

Abstract

Synth. Commun. 2006, 35, 169

NEW SYNTHESIS OF DONEPEZIL THROUGH PALLADIUM‐CATALYZED HYDROGENATION APPROACH

Chandrashekar R. Elati,1 Naveenkumar Kolla,1 Subrahmanyeswara Rao Chalamala,1 Pravinchandra J. Vankawala,1 Venkataraman Sundaram,1 Himabindu Vurimidi,2 and Vijayavitthal T. Mathad1

1Department of Research and Development, Dr. Reddy's Laboratories Ltd., IPD, Unit III, Bollaram, Hyderabad 502 325, Andhra Pradesh, India

2Institute of Science and Technology, J. N. T. University, Kukatpally, Hyderabad, Andhra Pradesh, India

Abstract

Synth. Commun. 2006, 35, 175

ASYMMETRIC INDUCTION FROM ETHYL LACTATE IN THE REDUCTION OF ACETOPHENONE TO PHENYLETHANOL

Stefan H. Hüttenhain

Fachhochschule Darmstadt, Fachbereich Chemie und Biotechnologie, Hochschulstrasse 2, Darmstadt 64289, Germany

Abstract

Synth. Commun. 2006, 35, 181

PREPARATION AND CHEMICAL BEHAVIOR OF 2‐(TERT‐BUTOXYCARBONYL) AMINO‐3‐BROMOMETHYL PYRIDINE, A NOVEL ALKYLATING AGENT

Mikhail Krasavin, Sergey Shkavrov, and Dmitry Kravchenko

Chemical Diversity Research Institute, 2a Rabochaya St., Khimki, Moscow Reg., Russia

Abstract

Synth. Commun. 2006, 35, 187

FACILE PREPARATION AND PURIFICATION OF MONO TERT‐BUTYL MALONATE

Vitali I. Tararov,1 Andrei Korostylev,1 Gerd König,2 and Armin Börner1,3

1Leibniz‐Institut für Organische Katalyse e.V., A.‐Einsteinstr. 29a, 18059 Rostock, Germany

2Ratiopharm GmbH, Ulm, Germany

3Institut für Chemie der Universität Rostock, Rostock, Germany

Abstract

Synth. Commun. 2006, 35, 193

SYNTHESIS OF N‐SUBSTITUTED 4,6‐DIMETHYL‐3‐CYANO‐2‐PYRIDONES UNDER MICROWAVE IRRADIATION

Dušan Mijin and Aleksandar Marinković

Department of Organic Chemistry, Faculty of Technology and Metallurgy, University of Belgrade, 11120 Belgrade, Serbia and Montenegro

Abstract

Synth. Commun. 2006, 35, 199

FIRST HIGHLY EFFICIENT SYNTHESIS OF BIS(ARYLMETHYLIDENE) PYRANONES MEDIATED BY LITHIUM PERCHLORATE

M. Saeed Abaee, Mohammad M. Mojtahedi, M. Mehdi Zahedi, and S. Mohammad Bolourtchian

Chemistry and Chemical Engineering Research Center of Iran, P.O. Box 14335‐186 Tehran, Iran

Abstract

Synth. Commun. 2006, 35, 207

MICROWAVE‐MEDIATED DEBROMINATION OF VICINAL‐DIBROMIDES

J. M. Khurana and A. Agrawal

Department of Chemistry, University of Delhi, Delhi 110007, India

Debromination of vicinal‐dibromides to E‐alkenes is reported using inorganic solid supports (silica gel or acidic alumina) under microwave irradiation.

Abstract

Synth. Commun. 2006, 35, 211

EFFICIENT METHOD FOR SILYLATION OF P‐NITROBENZYL‐2‐DIAZOACETOACETATE

Neera Tewari, Bishwa Prakash Rai, Hashim Nizar, and Shailendra Kumar Singh

Chemical Research Division, Ranbaxy Research Laboratories, Plot No. 20, Sector‐18, Udyog Vihar Industrial Area, Gurgaon 122 001, Haryana, India

Abstract

Synth. Commun. 2006, 35, 215

SYNTHESIS AND EVALUATION OF SUBSTITUTED PYRAZOLES: POTENTIAL ANTIMALARIALS TARGETING THE ENOYL‐ACP REDUCTASE OF PLASMODIUM FALCIPARUM

Sanjay Kumar,1 Gyanendra Kumar,1 Mili Kapoor,1 Avadhesha Surolia,1 and Namita Surolia2

1Molecular Biophysics Unit, Indian Institute of Science, Bangalore, India

2Molecular Biology and Genetics Unit, Jawaharlal Nehru Center for Advanced Scientific Research, Jakkur, Bangalore 560064, India

Abstract

Synth. Commun. 2006, 35, 227

COPPER(II) BROMIDE–CATALYZED IMINO DIELS–ALDER REACTION: SYNTHESIS OF PYRANO[3,2‐C]‐ AND FURO[3,2‐C]TETRAHYDROQUINOLINES

Abha Semwal and Sandip K. Nayak

Bio‐organic Division, Bhabha Atomic Research Centre, Mumbai 400085, India

Abstract

Synth. Commun. 2006, 35, 237

FACILE METHOD FOR STEREOSELECTIVE SYNTHESIS OF NEW CHIRAL (1R,4aR,8aR)‐1,3,4,4a,5,7,8,8a‐OCTAHYDRO‐2‐METHYLENE‐NAPHTHALENE‐6‐ONE‐1‐PROPANENITRILE, AN IMPORTANT PRECURSOR OF SOLANAPYRONES

Haijian Shi

College of Chemistry and Chemical Engineering, Key Laboratory of Material‐Oriented Chemical Engineering of Jiangsu Provience, Nanjing University of Technology, Nanjing 210009, China

A short stereoselective synthesis of new precursor of solanapyrone, using one‐pot hydrogenation/acetalization and Beckmann fragmentation as the key steps, is described.

Abstract

Synth. Commun. 2006, 35, 249

ACID‐PROMOTED RING OPENING OF α‐HYDROXYL CYCLOBUTANONES: A NOVEL AND FACILE ONE‐POT SYNTHESIS OF NITRILE DERIVATIVES

Xingxian Zhang1 and Weidong Z. Li2

1College of Pharmaceutical Sciences, Zhejiang University of Technology, Hangzhou, Zhejiang 310014, China

2National Laboratory of Applied Organic Chemistry and Institute of Organic Chemistry, Lanzhou University, Lanzhou, Gansu, China

A facile one‐pot synthesis of nitriles via a ring‐opening reaction of cyclobutanone adducts with hydroxylamine hydrochloride was developed.

Abstract

Synth. Commun. 2006, 35, 255

α‐CHLORINATION OF ACETOPHENONES USING 1,3‐DICHLORO‐5,5‐DIMETHYLHYDANTOIN

Zijin Xu, Deyan Zhang, and Xinzhuo Zou

Department of Chemistry, East China Normal University, 3663 Zhongshan Road (N), Shanghai 200062, China

A novel method for the synthesis of α‐chloroacetophenones using 1,3‐dichloro‐5,5‐dimethylhydantoin (DCDMH) and p‐toluenesulfonic acid in methanol at 30–35°C is described.

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