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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 36, 2006 - Issue 6
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Original Articles

Efficient Method for Synthesis of the Derivatives of 5‐Arylidene Barbituric Acid Catalyzed by Aminosulfonic Acid With Grinding

Ji‐Tai Li College of Chemistry and Environmental Science, Hebei University, Key Laboratory of Analytical Science and Technology of Hebei Province, Baoding, ChinaCorrespondence[email protected]
,
Hong‐Guang Dai College of Chemistry and Environmental Science, Hebei University, Key Laboratory of Analytical Science and Technology of Hebei Province, Baoding, China
,
Da Liu College of Chemistry and Environmental Science, Hebei University, Key Laboratory of Analytical Science and Technology of Hebei Province, Baoding, China
&
Tong‐Shuang Li College of Chemistry and Environmental Science, Hebei University, Key Laboratory of Analytical Science and Technology of Hebei Province, Baoding, China
Pages 789-794 | Received 15 Jul 2005, Published online: 16 Aug 2006
 
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Abstract

Aminosulfonic acid is an environmentally friendly catalyst. Grinding a mixture of aromatic aldehydes, barbituric acid, and H2NSO3H at room temperature (without any solvent) gave 5‐arylidene barbituric acid in high yields, providing a simple and efficient route to synthesis of these compounds.

Acknowledgments

Educational Ministry of China, Educational Department of Hebei Province (2001104), and Natural Science Foundation of Hebei Province (203107), China, supported the project.

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