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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 36, 2006 - Issue 9
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Original Articles

Rapid and Efficient Method for Acetylation of Alcohols and Phenols with Acetic Anhydride Catalyzed by Silica Sulfate

Ying Zhao Department of Chemistry, College of Chemistry and Environmental Science, Hebei University, Baoding, China
,
Li‐Bin Liu Department of Chemistry, College of Chemistry and Environmental Science, Hebei University, Baoding, China
,
Zhuo Chen Department of Chemistry, College of Chemistry and Environmental Science, Hebei University, Baoding, China
,
Tong‐Shuang Li Department of Chemistry, College of Chemistry and Environmental Science, Hebei University, Baoding, China
&
Tong‐Shou Jin Department of Chemistry, College of Chemistry and Environmental Science, Hebei University, Baoding, ChinaCorrespondence[email protected]
Pages 1221-1227 | Received 28 Jul 2005, Published online: 24 Feb 2007
 
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Abstract

A rapid and efficient method is described for acetylation of a series of alcohols and phenols with acetic anhydride catalyzed by silica sulfate solid acid at room temperature or at refluxing temperature in excellent yield.

Acknowledgments

The project was supported by the National Natural Science Foundation of China (29872011 and 29572039), Educational Ministry of China, Educational Department of Hebei Province (990104), and the Science and Technology Commission of Hebei Province.

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