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The catalyst‐ and solvent‐free Suzuki coupling reaction of sodium tetraphenylborate with hypervalent iodonium salts was achieved under microwave irradiation in the absence of a base. A convenient method for formation of carbon–carbon bonds afforded good yields in a short time.
Financial support from the Zhejiang Province Natural Science Foundation of China (Project Y404016) and Zhejiang Province Education Foundation of China (Project 20040569) is greatly appreciated.
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