Convenient Rearrangement Reaction of 2‐Chloroglycidic Esters by PPh₃: A New Synthetic Method of 3‐Chloro‐2‐keto Esters

Takuzo Komiyama Department of Material and Energy Science, Graduate School of Environmental Science, Okayama University, Okayama, Japan

Yutaka Takaguchi Department of Material and Energy Science, Graduate School of Environmental Science, Okayama University, Okayama, Japan

Sadao Tsuboi Department of Material and Energy Science, Graduate School of Environmental Science, Okayama University, Okayama, JapanCorrespondence[email protected]

Abstract

A convenient rearrangement reaction of 2‐chloroglycidic esters is reported. Treatment of 2‐chloroglycidic esters with PPh₃ under refluxing condition results in the formation of 3‐chloro‐2‐keto esters in good to reasonable yields.

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Convenient Rearrangement Reaction of 2‐Chloroglycidic Esters by PPh₃: A New Synthetic Method of 3‐Chloro‐2‐keto Esters

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Convenient Rearrangement Reaction of 2‐Chloroglycidic Esters by PPh3: A New Synthetic Method of 3‐Chloro‐2‐keto Esters

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Convenient Rearrangement Reaction of 2‐Chloroglycidic Esters by PPh₃: A New Synthetic Method of 3‐Chloro‐2‐keto Esters