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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 36, 2006 - Issue 24
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Original Articles

New Route for the Synthesis of Pyrazole, Triazole, Triazine, and Triazepine Derivatives

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Pages 3647-3653 | Received 16 Aug 2005, Published online: 01 Dec 2006
 

Abstract

N,N′‐Diphenylpiperidine‐1‐carbohydrazonamide 1 was prepared and treated with halo compounds, active nitriles, diethylhy malonate, ketones, CS2, phenylisocyanate, phenylisothiocyanate, LR, ethyl 2‐cyano‐3,13‐dithiomethylacetate, and benzylidenenitriles to give the corresponding triazines 2–4, pyrazoles 5 and 6, triazoles 7, 8, and 10, triazaphosphole 11, and triazepines 12 14, respectively.

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