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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 37, 2007 - Issue 1
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Original Articles

Synthesis and Structure of Novel Disulfide(trisulfide)‐Containing Thiophenes

Shi‐Ren Deng Department of Chemistry, Wuhan University, Wuhan, China
,
Tao Wu Department of Chemistry, Shantou University, Shantou, China
,
Gao‐Qiang Hu Department of Chemistry, Wuhan University, Wuhan, China
,
Dan Li Department of Chemistry, Shantou University, Shantou, China
,
Yun‐Hong Zhou Department of Chemistry, Wuhan University, Wuhan, China
&
Zao‐Ying Li Department of Chemistry, Wuhan University, Wuhan, ChinaCorrespondence[email protected]
Pages 71-78 | Received 09 Apr 2006, Published online: 25 Jul 2007
 
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Abstract

A novel trisulfide‐containing thiophene, 1,5‐dihydrothieno[3,4‐e][1,2,3]trithiepine (5), and a disulfide analogue, 1,4‐dihydrothieno[3,4‐d][1,2]dithiine (4), were designed and synthesized. All the compounds were characterized by FT‐IR, NMR, Raman, MS, and elemental analysis, some of which were confirmed by single‐crystal structure analysis. The designed molecules have potential usage as the cathode material for batteries.

Acknowledgment

We gratefully acknowledge financial support from the National Natural Science Foundation of China (No. 29833090).

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