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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 36, 2006 - Issue 23
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Abstracts

Graphical Abstracts

Pages i-vii | Published online: 24 Nov 2006
 

Abstract

Graphical Abstract Section

Abstract

Synth. Commun. 2006, 36, 3461

A CLOSER LOOK AT THE HYDROIODINATION OF PROPIOLIC ACID

James P. Donahue

Department of Chemistry, Tulane University, New Orleans, LA, USA

The product isolated from the hydroiodination of propiolic acid is found to dependent upon the specific reaction conditions employed.

Abstract

Synth. Commun. 2006, 36, 3473

RECYCLABLE AND LIGANDLESS SUZUKI COUPLING CATALYZED BY CARBON NANOTUBE‐SUPPORTED PALLADIUM NANOPARTICLES SYNTHESIZED IN SUPERCRITICAL FLUID

Horng‐Bin Pan, Clive H. Yen, Byunghoon Yoon, Masaki Sato, and Chien M. Wai

Department of Chemistry, University of Idaho, Moscow, Idaho, USA

Carbon nanotube‐supported palladium nanoparticles prepared by a supercritical fluid deposition method show high activities for catalyzing Suzuki coupling reactions and the catalysts can be recycled and reused at least six times without losing activity.

Abstract

Synth. Commun. 2006, 36, 3479

ONE‐POT SYNTHESIS OF OXIME DERIVATIVES OF 1,3‐DIPHENLYPYRAZOLE‐4‐CARBOXALDEHYDES FROM ACETOPHENONE PHENYLHYDRAZONES USING VILSMEIER–HAACK REAGENT

Om Prakash,1 Kamaljeet Pannu,1 Rajesh Naithani,1 and Harpreet Kaur2

1Department of Chemistry, Kurukshetra University, Kurukshetra, India

2Department of Pharamaceutical Sciences, Wayne State University, Detroit, MI, USA

A one‐pot synthesis of oxime derivatives 3a3f of 1‐phenyl‐3‐arylpyrazole‐4‐carboxaldehydes has been accomplished by the Vilsmeier–Haack reaction of acetophenone phenylhydrazones 1a1f under a new workup procedure.

Abstract

Synth. Commun. 2006, 36, 3487

CONVENIENT SYNTHESIS OF N,N′‐BIS‐PROTECTED‐3,3′‐DIIODO‐2,2′‐BIINDOLES

Sudipta Roy and Gordon W. Gribble

Department of Chemistry, Dartmouth College, Hanover, New Hampshire, USA

Abstract

Synth. Commun. 2006, 36, 3493

FACILE ONE‐POT SYNTHESIS OF 2‐ARYL‐SUBSTITUTED NITRILES AND 2‐ARYL‐3‐KETO NITRILES VIA BENZYNE REACTION

Sukanta Kamila, Benjamin Koh, and Edward R. Biehl

Southern Methodist University, Dallas, TX, USA

Abstract

Synth. Commun. 2006, 36, 3509

SELECTIVE APICAL BROMINATION OF DIAMANTANE AND CONVERSION TO THE DIHYDROXY AND DICARBOXYLIC ACID DERIVATIVES

Matthew C. Davis1 and Shenggao Liu2

1Chemistry and Materials Division, Michelson Laboratory, Naval Air Warfare Center, China Lake, CA, USA

2MolecularDiamond Technologies, Chevron Technology Ventures, LLC, Richmond, CA, USA

Abstract

Synth. Commun. 2006, 36, 3515

SYNTHESIS OF A THIOPHENE‐BASED NONLINEAR OPTICAL CHROMOPHORE

Matthew C. Davis, Richard A. Hollins, and Brad Douglas

Chemistry and Materials Division, Michelson Laboratory, Naval Air Warfare Center, China Lake, CA, USA

The chromophore was synthesized in eight steps in 38% overall yield.

Abstract

Synth. Commun. 2006, 36, 3525

SYNTHESIS OF 2‐OXO‐7‐SULFAMOYL‐2,3,4,5‐TETRAHYDRO‐1H‐BENZO [B]AZEPINES

Mikhail V. Dorogov,1 Sergey A. Ivanovsky,1 Maria Y. Khakhina,1 Dmitry V. Kravchenko,2 Sergey E. Tkachenko,3 and Alexandre V. Ivachtchenko3

1Ushinsky Yaroslavl State Pedagogical University, Yaroslavl, Russia

2Chemical Diversity Research Institute, Khimki, Moscow, Russia

3ChemDiv, Inc., San Diego, California, USA

Novel amide derivatives of 2‐оxo‐7‐sulfonyl‐2,3,4,5‐tetrahydro‐1H‐benzo[b]azepine were efficiently prepared starting from 2‐oxo‐2,3,4,5‐tetrahydro‐1H‐benzo[b]azepine.

Abstract

Synth. Commun. 2006, 36, 3537

PRACTICAL SYNTHESIS OF N‐ALKYL‐N‐ALKYLOXYCARBONYLAMINOMETHYL PRODRUG DERIVATIVES OF ACETAMINOPHEN, THEOPHYLLINE, AND 6‐MERCAPTOPURINE

Susruta Majumdar and Kenneth B. Sloan

Department of Medicinal Chemistry, University of Florida, Gainesville, FL, USA

Abstract

Synth. Commun. 2006, 36, 3549

REGIOSELECTIVE N‐ARYLATION OF SOME PYRIMIDINE AND PURINE NUCLEOBASES

Ali Khalafi‐Nezhad,1 Abdolkarim Zare,1 Abolfath Parhami,1 Mohammad Navid Soltani Rad,2 and Gholam Reza Nejabat1

1Department of Chemistry, College of Sciences, Shiraz University, Shiraz, Iran

2Department of Chemistry, College of Basic Sciences, Shiraz University of Technology, Shiraz, Iran

Abstract

Synth. Commun. 2006, 36, 3563

NEW PROTOCOL TO SYNTHESIZE SPIRO‐1,4‐DIHYDROPYRIDINES BY USING A MULTICOMPONENT REACTION OF CYCLOHEXANONE, ETHYL CYANOACETATE, ISATIN, AND PRIMARY AMINES UNDER MICROWAVE IRRADIATION

Farhad Hatamjafari

Department of Chemistry, Faculty of Science, Islamic Azad University‐Tonekabon Branch, Tonekabon, Iran

Abstract

Synth. Commun. 2006, 36, 3571

APPLICATION OF ALKALI METAL HYDROXIDES FOR THE PREPARATION OF GEM‐CHLOROPHENYLCYCLOPROPANES

Andrzej Jończyk, Hanna Karwowska, and Jolanta Furman

Faculty of Chemistry, Warsaw University of Technology, Warszawa, Poland

Abstract

Synth. Commun. 2006, 36, 3581

SYNTHESIS OF NEW QUINOLINE DERIVATIVES

Judit Tóth, Gábor Blaskó, András Dancsó, László Tőke, and Miklós Nyerges

Department of Organic Chemical Technology, Budapest University of Technology and Economics, Budapest, Hungary

Abstract

Synth. Commun. 2006, 36, 3591

ATYPICAL OXIDATION REACTION BY THIONYL CHLORIDE: EASY TWO‐STEP SYNTHESIS OF N‐ALKYL‐1,4‐DITHIINES

Alain Valla, Dominique Cartier, Frédéric Zentz, and Roger Labia

Chimie et Biologie des Substances Naturelles FRE 2125 CNRS 6, rue de l'Université, 29000 Quimper, France

Abstract

Synth. Commun. 2006, 36, 3599

KF/Al2O3‐MEDIATED N‐ALKYLATION OF AMINES AND NITROGEN HETEROCYCLES IN AND S‐ALKYLATION OF THIOLS

Firouz Matloubi Moghaddam, Seyedeh Maryam DokhtTaimoory, Hossein Ismaili, and Ghasem Rezanejade Bardajee

Department of Chemistry, Sharif University of Technology, Tehran, Iran

Different types of amines and thiols react smoothly with various alky halides in the presence of KF/Al2O3 to afford corresponding N‐alkylated amines and thioethers.

Abstract

Synth. Commun. 2006, 36, 3609

EFFICIENT AND MILD PROCEDURE FOR REDUCTIVE METHYLATION OF AMINES USING N‐METHYLPIPERIDINE ZINC BOROHYDRIDE

Heshmatollah Alinezhad, Mahmood Tajbakhsh, and Reza Zamani

Department of Chemistry, Mazandaran University, Babolsar, Iran

N‐Methylpiperidine zinc borohydride (ZBNMPP) is an efficient reagent for the reductive methylation of primary and secondary amines, giving the corresponding tertiary methylated amines in high yield.

Abstract

Synth. Commun. 2006, 36, 3617

EFFICIENT APPROACH FOR THE SYNTHESIS OF NOVEL FUNCTIONALIZED ISOXAZOLINES FROM LIMONENE

Amal Feddouli,1 My Youssef Ait Itto,1 Mustapha Ait Ali,1 Aïssa Hasnaoui1, and Abdelkhalek Riahi2

1Department of Chemistry, Faculty of Science‐Semlalia, BP 2390, Marrakech, Morocco

2Unity of research ≪Selective Reactions and Applications≫ NCSR, University of Rheims Champagne‐Ardenne, Rheims, France

Convenient and efficient synthesis of new isoxazolyl‐ketoacids from limonene is reported.

Abstract

Synth. Commun. 2006, 36, 3625

ZEOLITE‐CATALYZED ENVIRONMENTALLY FRIENDLY SYNTHESIS OF BENZIMIDAZOLE DERIVATIVES

Adrienn Hegedüs, Zoltán Hell, and Attila Potor

Department of Organic Chemical Technology, Budapest University of Technology and Economics, H‐1521, Budapest, Hungary

Abstract

Synth. Commun. 2006, 36, 3631

REACTIONS OF 6‐AMINOURACILS: THE FIRST SIMPLE, FAST, AND HIGHLY EFFICIENT SYNTHESIS OF BIS(6‐AMINOPYRIMIDONYL)METHANES (BAPMS) USING THERMAL OR MICROWAVE‐ASSISTED SOLVENT‐FREE METHODS

Javad Azizian,1 Mohammad R. Mohammadizadeh,1 Fatemeh Teimouri,2 Ali A. Mohammadi,1 and Ali R. Karimi1

1Chemistry Department, Shahid Beheshti University, Tehran, Iran

2Department of Chemistry, Science and Research Campus, Islamic Azad University, Tehran, Iran

Abstract

Synth. Commun. 2006, 36, 3639

RAPID SYNTHESIS OF NEW 5‐NITROIMIDAZOLES AS POTENTIAL ANTIBACTERIAL DRUGS VIA VNS PROCEDURE

Maxime D. Crozet, Vincent Rémusat, Christophe Curti, and Patrice Vanelle

Laboratoire de Chimie Organique Pharmaceutique, UMR–CNRS 6517, Faculté de Pharmacie, Marseille, France

Original 4‐arylsulfonylmethyl‐5‐nitroimidazoles were prepared by reacting four chloromethylaryl sulfones with 5‐nitroimidazole derivatives via a VNS reaction.

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