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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 37, 2007 - Issue 8
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Original Articles

Solvent‐Free Iodination of Arenes using Iodine–Silver Nitrate Combination

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Pages 1259-1265 | Received 03 Oct 2006, Published online: 12 Apr 2007
 

Abstract

A simple and environmentally safe general method of iodination of aromatic substrates under sovent‐free conditions using the I2/AgNO3 combination in a solid state is reported. Both activated and deactivated aromatic compounds afford the respective aryl iodides in generally high yields (80–90%).

Acknowledgments

The authors thank Victor D. Filimonov (Department of Organic Chemistry, Tomsk Polytechnic University) for helpful discussion. V. V. Z. is thankful to the National Science Foundation (NSF/CHE‐0353541 and NSF‐MRI award CHE 0416157) for partial support of this research.

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