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Abstract
Graphical Abstract Section
Abstract
Synth. Commun. 2007, 37, 3697
SYNTHETIC ACCESS TO NEW PYRIDONE DERIVATIVES THROUGH THE ALKYLATION REACTIONS OF HYDROXYPYRIDINES WITH EPOXIDES
Ahmet Kocak, Sultan Kurbanli, and Sait Malkondu
Faculty of Science and Arts, Department of Chemistry, University of Selcuk, Konya, Turkey
Abstract
Synth. Commun. 2007, 37, 3709
NEW CONVENIENT REAGENTS FOR CHEMOSELECTIVE N-ALKOXYCARBONYLATION OF (S)-ISOSERINE: APPLICATION IN the ISEPAMICIN SYNTHESIS
Konstantin Doktorov, Velichko Tarpanov, and Pepa Mechkarova
Institute of Organic Chemistry with Centre of Phytochemistry, Bulgarian Academy of Science, Sofia, Bulgaria
Abstract
Synth. Commun. 2007, 37, 3719
NOVEL METHOD FOR THE SYNTHESIS OF [1,2,4]TRIAZINO[4,3-C]QUINAZOLINE SYSTEM
Sergey I. Kovalenko,1 Alexander V. Karpenko,1 Oksana V. Krivoshey,1 Svetlana V. Shishkina,2 and Oleg V. Shishkin2
1Department of Pharmaceutical Chemistry, Zaporozhye State Medical University, Zaporozhye, Ukraine
2STC Institute for Single Crystals, National Academy of Sciences of Ukraine, Kharkov, Ukraine
Abstract
Synth. Commun. 2007, 37, 3729
STUDIES ON THE SELECTIVE REDUCTION OF THE AMIDE LINK OF ACYCLIC AND MACROCYCLIC AMIDOKETALS: UNEXPECTED CLEAVAGE AND TRANS-ACETALIZATION WITH RED-AL®
Radouane Affani and Denise Dugat
Laboratoire SEESIB (Synthèse et Etude de Systèmes à Intérêt Biologique), Université Blaise Pascal de Clermont-Ferrand, Aubière, France
Abstract
Synth. Commun. 2007, 37, 3741
Novel Atom-Economic Nitration of Benzene with a Nitrogen Dioxide–Oxygen System using Cocatalyst of Solid Oxides and Lanthanide(III) Metal Triflates
Xiaohua Du, Xiaoqing Li, and Zhenyuan Xu
State Key Laboratory Breeding Base of Green Chemistry–Synthesis Technology, Zhejiang University of Technology, Hangzhou, China
Abstract
Synth. Commun. 2007, 37, 3751
SAMARIUM TRIIODIDE–CATALYZED FORMATION OF MANNICH-TYPE PRODUCTS BY AMIDOALKYLATION OF 1,3-DICARBONYL COMPOUNDS
Xiaoxia Wang, Hui Mao, Yan yu, Xiudan Zhu, and Chunlan Zhu
Zhejiang Key Labortary for Reactive Chemistry on Solid Surfaces, College of Chemistry and Life Scienes, Zhejiang Normal University, Jinhua, China
Abstract
Synth. Commun. 2007, 37, 3759
Convenient Synthesis of Aryl Ferrocenyl Ketone via Palladium‐Catalyzed Carbonylation Coupling
Dong Yang,1 Zenglu Liu,2 Ying Li,1 and Baohua Chen1
1State Key Laboratory of Applied Organic Chemistry, Lanzhou University China, Lanzhou, China
2Pharmacy College of Shanghai Jiao Tong University, Shanghai, China
Abstract
Synth. Commun. 2007, 37, 3767
Efficient One-pot Synthesis of 2-Amino-4,6-diarylbenzene-1,3-dicarbonitrile under Solvent-free Conditions
Liangce Rong,1,2 Hongxia Han,1 Fang Yang,1 Hao Yao,1 Hong Jiang,2 and Shujiang Tu,1,2
1Department of Chemistry, Xuzhou Normal Univeristy, Xuzhou, Jiang Su, China
2Key laboratory of Biotechnology for Medicinal Plant, Xuzhou, Jiangsu, China
A facile parallel synthesis of 2-amino-4,6-diarylbenzene-1,3-dicarbonitrile derivatives via one-pot reaction of aromatic aldehydes, aromatic ketone, malononitrile under solvent-free conditions has been developed. This new protocol has the advantages of shorter time, higher yields, lower cost, and environmental friendliness.
Abstract
Synth. Commun. 2007, 37, 3773
Novel Synthetic Route of (2S)‐6‐Fluoro‐4‐oxo‐3,4‐dihydro‐2H‐chromene‐2‐carboxylic Acid
Hua-Jie Yuan, Shan Quian, Li Hai, Yao-Yao Chen, and Yong Wu
Key Laboratary of Drug Targeting of Education Ministry, West China School of Pharmacy, Sichuan University, Chengdu, Sichuan, China
(2S)‐6‐Fluoro‐4‐oxo‐3,4‐dihydro‐2H‐chromene‐2‐carboxylic acid, a key intermediate of Fidarestat, was synthesized from natural chiral pool D‐mannitol.
Abstract
Synth. Commun. 2007, 37, 3779
Synthesis biological evaluation of new 4-deacety-1,7,9-trideoxy-10-oco paclitaxel via sinenxan A
Huixia Du,1 Meng Zhang,1 Dali Yin,1 Yan Li,2 and Xiaoguang Chen2
Abstract
Department of Medicinal Chemistry, Institute of Materia Medica, Peking Union Medical College and Chinese Academy of Medical Science, Beijing, China
Department of Pharmacology, Institute of Materia Medica, Peking Union Medical College and Chinese Academy of Medical Science, Beijing, China
A new 1,7,9-trideoxy-4-deacety-10-oxopaclitaxel (1) was synthesized in 21 steps via sinenxan A and evaluated in vitro for cytotoxicity against human cancer cell lines.
Abstract
Synth. Commun. 2007, 37, 3793
Practical Synthesis Of Structurally Important Spirodiamine Templates
Fei‐Yu Tang, Li‐Qiang Qu, Yan Xu, Ru‐Jian Ma, Shu‐Hui Chen, and Ge Li
A general, concise four‐step synthetic sequence for the preparation of the spiro‐diamine templates is described herein.
Abstract
Synth. Commun. 2007, 37, 3801
Unexpected Rearrangement in the Reaction of 7-Mercapto-4-methylcoumarin with 1-Mono- and 1,1-Dimethyl Propargyl Alcohols
Shiqing Xu, Xin Yan, Qian Zhang, Peng Xia, and Ying Chen
Department of Medicinal Chemistry, School of Pharmacy, Fudan University, Shanghai, China The reaction of 7-mercapo-4-methylcoumarin (4) with 1-mono- and 1,1-dimethyl propargyl alcohols in H3PO4 afforded the corresponding β-(7-coumarinthio)ketones with a rearrangement of the carbon chain of propargyl.
Abstract
Synth. Commun. 2007, 37, 3809
PALLADIUM-CATALYZED KUMADA REACTION EMPLOYING AMINOPHOSPHINE AS LIGAND
Lin Zhang, Jiang Cheng, Weiwei Zhang, Baoda Lin, Changduo Pan, and Jing Chen
College of Chemistry and Material Engineering, Wenzhou University, Wenzhou, China
Abstract
Synth. Commun. 2007, 37, 3815
SYNTHESIS OF 3-ARYL-5-T-BUTYLSALICYLALDEHYDES AND THEIR CHIRAL SCHIFF BASE COMPOUNDS
Hai-Bin Liu,1 Mei Wang,1 Ying Wang,1 Qiang Gu,1 and Li-Cheng Sun1,2
1State Key Laboratory of Fine Chemicals, Dalian University of Technology, Dalian, Liaoning, China
2School of Chemical Science and Engineering, Royal Institute of Technology, Stockholm, Sweden
Abstract
Synth. Commun. 2007, 37, 3827
YTTERBIUM PERFLUOROOCTANESULFONATE CATALYZED SYNTHESIS OF 1,5-BENZODIAZEPINE DERIVATIVES IN FLUOROUS SOLVENTS
Wen-Bin Yi and Chun Cai
Chemical Engineering College, Nanjing University of Science and Technology, Nanjing, China
Abstract
Synth. Commun. 2007, 37, 3835
Solid-State Photodimerization of 1,2-bis(5′-Pyrimidyl)ethene
Eric Bosch,1 Julie M. Matheny,1 and Nigam Rath2
1Depatment of Chemistry, Missouri State University, Springfield, Missouri, USA
2Department of Chemistry, University of Missouri, St. Louis, Missouri, USA
Abstract
Synth. Commun. 2007, 37, 3841
NEW PHOSPHONATE REAGENTS FOR ALDEHYDE HOMOLOGATION
Richard J. Petroski
United States Department of Agriculture, Agricultural Research Service, National Center for Agricultural Utilization Research, Crop Bioprotection Research Unit, Peoria, Illinois, USA Using these reagents led to a two-step aldehyde homologation cycle (condensation and deprotection), and overall yields ranged from 71% to 84%.
Abstract
Synth. Commun. 2007, 37, 3855
COMPARISON OF IODINATION OF METHOXYLATED BENZALDEHYDES AND RELATED COMPOUNDS USING IODINE/SILVER NITRATE AND IODINE/PERIODIC ACID
Bruce A. Hathaway, Kristen L. White, and Mark E. McGill
Department of Chemistry, Southeast Missouri State University, Cape Girardeau, Missouri, USA
Abstract
Synth. Commun. 2007, 37, 3861
Synthesis and characterization of novel quaternary ammonium RAFT agents
Austin Samakande, Ronald D. Sanderson, and Patrice C. Hartmann
UNESCO Associated Centre for Macromolecules, Department of Chemistry and Polymer Science, Univrsity of Stellenbosch, Matieland, South Africa
Abstract
Synth. Commun. 2007, 37, 3873
Convenient Synthesis of Tributylsilyl Methacrylate
David Mancardi,1 Michèle Sindt,1 Jean‐Michel Paul,2 and Jean‐Luc Mieloszynski1
1Laboratory of Chemistry and Methodology for the Environment (LCME), Paul Verlaine‐Metz University, Metz, France 2Arkema, Research and Development Centre (CRDE), Saint Avold, France
Abstract
Synth. Commun. 2007, 37, 3879
New Access to Organoacyloxytrialkylsilanes
David Mancardi,1 Michèle Sindt,1 Jean‐Michel Paul,2 and Jean‐Luc Mieloszynski1
1Laboratory of Chemistry and Methodology for the Environment (LCME), Paul Verlaine‐Metz University, Metz, France 2Arkema, Research and Development Centre (CRDE), Saint Avold, France
