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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 38, 2008 - Issue 2
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Original Articles

Ionic‐Liquid‐Supported Total Synthesis of Sansalvamide A Peptide

Ling Chen Center for Drug Discovery and Design, State Key Laboratory of Drug Research, Shanghai Institute of Materia Medica, Shanghai Institutes for Biological Sciences, and Chinese Academy of Sciences, Shanghai, China
,
Mingfang Zheng Center for Drug Discovery and Design, State Key Laboratory of Drug Research, Shanghai Institute of Materia Medica, Shanghai Institutes for Biological Sciences, and Chinese Academy of Sciences, Shanghai, China
,
Yu Zhou Center for Drug Discovery and Design, State Key Laboratory of Drug Research, Shanghai Institute of Materia Medica, Shanghai Institutes for Biological Sciences, and Chinese Academy of Sciences, Shanghai, China; School of Pharmaceutical Engineering, Shenyang Pharmaceutical University, Shenyang, Liaoning, China
,
Hong Liu Center for Drug Discovery and Design, State Key Laboratory of Drug Research, Shanghai Institute of Materia Medica, Shanghai Institutes for Biological Sciences, and Chinese Academy of Sciences, Shanghai, ChinaCorrespondence[email protected]
&
Hualiang Jiang Center for Drug Discovery and Design, State Key Laboratory of Drug Research, Shanghai Institute of Materia Medica, Shanghai Institutes for Biological Sciences, and Chinese Academy of Sciences, Shanghai, China; School of Pharmacy, East China University of Science and Technology, Shanghai, China
Pages 239-248 | Received 20 Jun 2006, Published online: 18 Jan 2008
 
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Abstract

A facile and efficient total synthesis of bioactive sansalvamide A peptide has been accomplished, including the‐ionic‐liquid supported method and final PyBOP‐promoted ring closure.

Acknowledgments

We gratefully acknowledge generous support from the National Natural Science Foundation of China (Grants 20372069, 29725203, and 20472094), the Key Technologies R&D Program from CAS (Grants 2005BA711A01), and the 863 Hi‐Tech Program of China (Grants 2006AA020402 and 2006AA020602).

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