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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 38, 2008 - Issue 2
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Original Articles

Direct Iodination of Monosubstituted Aryl Acetylenes and Acetylenic Ketones

, , &
Pages 225-231 | Received 22 Mar 2007, Published online: 18 Jan 2008
 

Abstract

Monosubstituted acetylenes were iodinated to form iodoacetylenes under simple conditions. Reaction of aryl acetylenes with molecular iodine in the presence of 4‐dimethylaminopyridine (DMAP) gave the desired products in good to excellent yields. Iodination of aryl acetylenic ketones using K2CO3 as base was also described.

Acknowledgments

We express our appreciation to the National Natural Science Foundation of China (20776114) and Program of NCET (060551).

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