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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 38, 2008 - Issue 2
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Abstracts

Graphical Abstracts

Pages 155-161 | Published online: 18 Jan 2008
 

Abstract

Graphical Abstract Section

Abstract

Synth. Commun. 2008, 38, 162

CONCISE AND EFFICIENT SYNTHESIS OF HIGHLY POTENT AND SELECTIVE DIPEPTIDYL PEPTIDASE II INHIBITORS

M. Abdul Rasheed, Rambabu Namala, Narendra Manne, Sreelatha Vanjivaka, Ravi Dhamjewar, and Gopalan Balasubramanian

Matrix Laboratories, Hyderabad, India

Abstract

Synth. Commun. 2008, 38, 170

MILD AND HIGHLY EFFICIENT STEREOSELECTIVE SYNTHESIS OF 2,3-UNSATURATED GLYCOPYRANOSIDES USING LA(NO3)3 · 6H2O AS A CATALYST: FERRIER REARRANGEMENT

N. Suryakiran, S. Malla Reddy, M. Srinivasulu, and Y. Venkateswarlu

Organic Chemistry Division I, Natural Products Laboratory, Indian Institute of Chemical Technology, Hyderabad, India

Abstract

Synth. Commun. 2008, 38, 177

FACILE TERT-BUTOXYCARBONYLATION OF ALCOHOLS, PHENOLS, AND AMINES USING BICL3 AS A MILD AND EFFICIENT CATALYST

N. Suryakiran, P. Prabhakar, and Y. Venkateswarlu

Organic Chemistry Division I, Natural Products Laboratory, Indian Institute of Chemical Technology, Hyderabad, India

Abstract

Synth. Commun. 2008, 38, 186

FERROUS SULFIDE/AQUEOUS AMMONIA: SIMPLE, EFFICIENT, AND CHEMOSELECTIVE REAGENT FOR THE CONVERSION OF AROMATIC AZIDE TO AMINE

Amol V. Gadakh and Bhausaheb K. Karale

Research and Postgraduate Department of Chemistry, S. S. G. M. College, University of Pune, Kopargaon, India

Abstract

Synth. Commun. 2008, 38, 192

PREPARATION OF MIXED CARBAMIC/DITHIOCARBAMIC ANHYDRIDES VIA SILYL CARBAMATES OR SILYL DITHIOCARBAMATES

Ferenc Kardon, Mária Mörtl, and Gábor Magyarfalvi

Institute of Chemistry, Eötvös Loránd University, Budapest, Hungary

Abstract

Synth. Commun. 2008, 38, 200

SYNTHESIS OF NEW (4-ACETONYLIDENE-2,6,8,9-TETRAMETHYL-7H-IMIDAZO[1,5,4-E,F][1,5]BENZODIAZEPINE) DERIVATIVES

Abdellatif El Kihel,1 Mustapha Ahbala,1 Abdelkrim Mouzdahir,1 Naima Snader,1 El Mokhtar Essassi,2 Patrick Bauchat,3 and Renée Danion-Bougot3

1Faculté des Sciences, Laboratoire de Chimie BioOrganique, El Jadida, Maroc

2Faculté des Sciences, Laboratoire de Chimie Organique Hétérocyclique, associé au CNCPRST, Rabat, Maroc

3Synthèse et Electrosynthèse Organiques, Université de Rennes I, Rennes Cédex, France

Abstract

Synth. Commun. 2008, 38, 205

RAPID RING-OPENING REACTIONS OF EPOXIDES USING MICROWAVE IRRADIATION

Christian Torborg,1 David D. Hughes,1 Richard Buckle,2 Mathew W. C. Robinson,2 Mark C. Bagley,1 and Andrew E. Graham2

1School of Chemistry, Cardiff University, Cardiff, Wales, U.K.

2Department of Chemistry, University of Wales Swansea, Swansea, U.K.

Abstract

Synth. Commun. 2008, 38, 212

ALTERNATIVE, HIGH-YIELD SYNTHESIS OF (E)-4-OXONON-2-ENOIC ACID FROM 2-METHOXYFURAN

Ahmet Maras,1 Ahmet Altay,1 and Roberto Ballini2

1Faculty of Arts and Sciences, Department of Chemistry, Ataturk University, Erzurum, Turkey

2Dipartimento di Scienze Chimiche dell'Università, Camerino, Italy

Abstract

Synth. Commun. 2008, 38, 217

ONE-POT SYNTHESIS OF 4,6-DIARYL-2-OXO-1,2-DIHYDROPYRIDINE-3-CARBONITRILES VIA THREE-COMPONENT CYCLOCONDENSATION UNDER SOLVENT-FREE CONDITIONS

Liangce Rong,1,2 Hongxia Han,1 Hong Jiang,1 Daqing Shi,1,2 and Shujiang Tu1,2

1Department of Chemistry, Xuzhou Normal University, Jiangsu, Xuzhou, China

2Key Laboratory of Biotechnology for Medical Plant, Jiangsu, Xuzhou, China

An efficient and facile synthesis of 4,6-diaryl-2-oxo-1,2-dihydropyridine-3-carbon itriles via three-component cyclocondensation from aromatic aldehydes, aromatic ketones, and 2-cyanoacetamide under solvent-free conditions is described. The mild reaction conditions, simple protocol, and clean reaction make this protocol practical and economically attractive.

Abstract

Synth. Commun. 2008, 38, 225

DIRECT IODINATION OF MONOSUBSTITUTED ARYL ACETYLENES AND ACETYLENIC KETONES

Ling-Guo Meng, Pei-Jie Cai, Qing-Xiang Guo, and Song Xue

Department of Chemistry, University of Science and Technology of China, Hefei, China

Abstract

Synth. Commun. 2008, 38, 232

EFFICIENT DMF-PROMOTED SOLVENTLESS HYDROLYSIS OF EPOXIDES WITH EQUIMOLAR AMOUNT OF H2O, AFFORDING 1,2-DIOLS

Jia-Li Jiang,1,2 Zhuo Xiu,1 and Ruimao Hua1

1Department of Chemistry, Tsinghua University, Beijing, China

2Medical Department, Shunde Polytechnic, Foshan, China

Abstract

Synth. Commun. 2008, 38, 239

IONIC-LIQUID-SUPPORTED TOTAL SYNTHESIS OF SANSALVAMIDE A PEPTIDE

Ling Chen,1 Mingfang Zheng,1 Yu Zhou,1,2 Hong Liu,1 and Hualiang Jiang1,3

1Center for Drug Discovery and Design, State Key Laboratory of Drug Research, Shanghai Institute of Materia Medica, Shanghai Institutes for Biological Sciences, and Chinese Academy of Sciences, Shanghai, China

2School of Pharmaceutical Engineering, Shenyang Pharmaceutical University, Shenyang, Liaoning, China

3School of Pharmacy, East China University of Science and Technology, Shanghai, China

A facile and efficient total synthesis of bioactive sansalvamide A peptide has been accomplished, including the-ionic-liquid-supported method and final PyBOP-promoted ring closure.

Abstract

Synth. Commun. 2008, 38, 249

EFFICIENT SYNTHESIS OF 1-ARYL-1H-INDAZOLE DERIVATIVES VIA COPPER (I)-CATALYZED INTRAMOLECULAR AMINATION REACTION

Rui Liu, Yongming Zhu, Liena Qin, and Shunjun Ji

College of Pharmacy, Soochow University, Suzhou, China

A copper(I)‐catalyzed intramolecular amination reaction under the condition of [CuI/KOH/1,4‐dioxane/105°C] for the preparation of 1‐aryl‐1H‐indazole derivatives was described. The method was applied to a wide scope of substrates and afforded indazole products in high yields.

Abstract

Synth. Commun. 2008, 38, 255

UNEXPECTEDLY HIGH ACTIVITY OF ZN(OTF)2 · 6H2O IN CATALYTIC FRIEDEL–CRAFTS ACYLATION REACTION

Fei he,1 Huayue wu,1 Jiuxi chen,1 and Weike su1,2

1College of Chemistry and Materials Science, Wenzhou University, Wenzhou, China

2College of Pharmaceutical Sciences, Zhejiang University of Technology, Zhejiang Key Laboratory of Pharmaceutical Engineering, Hangzhou, China

Zn(OTf)2 · 6H2O was used to promote Friedel–Crafts acylation of aromatics. The work describes the high activity and efficiency of Zn(OTf)2 · 6H2O in acylation of aromatics, and the catalyst has surpassed most metal triflates in dispensing when dried at high temperature under vacuum before use.

Abstract

Synth. Commun. 2008, 38, 265

FACILE SYNTHESIS OF N-ACYLSULFONAMIDE IN THE PRESENCE OF SILICA CHLORIDE (SIO2-CL) BOTH UNDER HETEROGENEOUS AND SOLVENT-FREE CONDITIONS

Ahmad Reza Massah, Ahmad Reza Momeni, Mina Dabagh Hamid Aliyan, and Hamid Javaherian Naghash

Department of Chemistry, Islamic Azad University, Shahreza Branch, Shahreza, Isfahan, Iran

Abstract

Synth. Commun. 2008, 38, 274

ISOCYANIDE-CATALYZED REACTION OF TETRACYANOETHYLENE AND ACTIVATED 1,3-DICARBONYL CH-ACID COMPOUNDS: A RAPID AND EFFICIENT SYNTHESIS OF PYRAN ANNULATED HETEROCYCLIC SYSTEMS

Ahmad Shaabani, Ali Hossein Rezayan, Afshin Sarvary, and Abbas Rahmati

Department of Chemistry, Shahid Beheshti University, Tehran, Iran

Abstract

Synth. Commun. 2008, 38, 282

ADDITIVE-FREE THIOLYSIS OF EPOXIDES IN WATER: A GREEN AND EFFICIENT REGIOSELECTIVE PATHWAY TO β-HYDROXY SULFIDES

M. Saeed Abaee1, Mohammad M. Mojtahedi,1 Hassan Abbasi,1 and Ensieh R. Fatemi2

1Chemistry and Chemical Engineering Research Center of Iran, Tehran, Iran

2Department of Chemistry, Islamic Azad University, Saveh Campus, Saveh, Iran

Room-temperature ring opening of various epoxides with aromatic thiols was carried out in water in the absence of any Lewis acid or additive. High yields of β-hydroxy sulfides with excellent regioselectivity were obtained under very environmentally friendly conditions.

Abstract

Synth. Commun. 2008, 38, 290

MONTMORILLONITE K10 CLAY: AN EFFICIENT CATALYST FOR HANTZSCH SYNTHESIS OF 1,4-DIHYDROPYRIDINE DERIVATIVES

A. Moshtaghi Zonouz and S. Baradaran Hosseini

Faculty of Science, Chemistry Department, Azarbaijan University of Tarbiat Moallem, Tabriz, Iran

Abstract

Synth. Commun. 2008, 38, 297

FACILE AND EFFICIENT ONE-POT PROTOCOL FOR SYNTHESIS OF 5-PHENYL-1,4-BENZODIAZEPINE-2-ONE DERIVATIVES

Javad Safaei-Ghomi and Alireza Hatami

Faculty of Science, Department of Chemistry, University of Kashan, Kashan, Iran

Abstract

Synth. Commun. 2008, 38, 303

CONVENIENT PREPARATION OF N-MALEOYL AMINO ACID SUCCINIMIDO ESTERS USING N-TRIFLUOROACETOXYSUCCINIMIDE

Michael J. Paterson1 and Ian M. Eggleston2

1Maternal and Child Health Sciences, Ninewells Hospital and Medical School, University of Dundee, Dundee, U.K.

2Department of Pharmacy and Pharmacology, University of Bath, Bath, U.K.

One-pot cyclization and esterification of maleamic acid using N-trifluoroacetoxysuccinimide provide to N-maleoyl amino acid succinimido ester derivatives.

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