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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 38, 2008 - Issue 7
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Original Articles

Solvent‐Free Aerobic Chemoselective Oxidation of β‐Ionone catalyzed by N‐Hydroxyphthalimide/Co(acac)2

Nian‐hua Gong School of Chemistry and Chemical Engineering, Central South University, Changsha, China
,
Rui‐Ren Tang School of Chemistry and Chemical Engineering, Central South University, Changsha, ChinaCorrespondence[email protected]
,
Ya‐ping Zhou School of Chemistry and Chemical Engineering, Central South University, Changsha, China
&
Hai‐feng Xu School of Chemistry and Chemical Engineering, Central South University, Changsha, China
Pages 1020-1027 | Received 12 May 2007, Published online: 12 Mar 2008
 
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Abstract

β‐Ionone was oxidized with O2 under solvent‐free conditions catalyzed by an N‐hydroxyphthalimide/Co(acac)2 system in mild conditions with high conversion and excellent selectivity to oxo‐β‐ionone or 5,6‐epoxy‐β‐ionone in different reaction conditions, respectively.

Acknowledgments

Financial support from the National Natural Science Foundation of China (No. 50573019) is gratefully acknowledged.

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