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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 38, 2008 - Issue 16
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Original Articles

Oxidative Bromination of Aromatic Compounds Using O-Iodoxybenzoic Acid with Tetraethylammonium Bromide

, &
Pages 2814-2819 | Received 01 Dec 2007, Published online: 25 Aug 2010
 

Abstract

A mild and selective procedure for the bromination of activated arenes using o-iodoxybenzoic acid and tetraethylammonium bromide is presented. The reactions were carried out at room temperature and gave moderate to excellent yields.

ACKNOWLEDGMENT

Authors thank the University Grants Commission (UGC), India, for financial support.

Notes

a Reactions were performed on a 5 mmol scale using 1.1 equiv. of IBX with TEAB. Reactions were monitored by TLC and GC analysis on 5% OV-17 (6′, 1/8″) column and FID detector.

b Isolated yields.

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