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Abstract
Graphical Abstract Section
Abstract
Synth. Commun. 2008, 38, 1498
APPLICATION OF HIGHLY EFFICIENT, RECYCLABLE ORGANIC–INORGANIC HYBRID MATERIAL IMMOBILIZED PALLADIUM CATALYST IN AMINE‐ AND PHOSPHINE‐FREE SUZUKI–MIYAURA REACTION
Liyuan Zhang,1 Lei Wang,1,2 Hongji Li,1 and Pinhua Li1
1Department of Chemistry, Huaibei Coal Teachers College, Huaibei, Anhui, China
2State Key Laboratory of Organometallic Chemistry, Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences, Shanghai, China
Abstract
Synth. Commun. 2008, 38, 1512
EFFICIENT SYNTHESIS OF CINACALCET HYDROCHLORIDE
Gopinathenpillai Bijukumar, Biswas Maloyesh, Bhirud Shekhar Bhaskar, and Agarwal Rajendra
Chemical Process Research and Development, Research and Development Centre, Macleods Pharmaceuticals Ltd., Mumbai, India
Abstract
Synth. Commun. 2008, 38, 1518
SbCl3 AS A HIGHLY EFFICIENT CATALYST FOR THE ACETYLATION OF ALCOHOLS, PHENOLS, AND AMINES UNDER SOLVENT‐FREE CONDITIONS
Asish K. Bhattacharya, Mamadou A. Diallo, and Krishna N. Ganesh
Combi Chem‐Bio Resource Centre and Division of Organic Chemistry, National Chemical Laboratory, Pune, India
A mild, efficient, and expeditious synthetic protocol has been developed for the protection of alcohols, phenols, and amines as acetates in excellent yields under solvent‐free conditions using acetic anhydride catalyzed by antimony trichloride.
Abstract
Synth. Commun. 2008, 38, 1527
EFFICIENT RING OPENING OF AZIRIDINES WITH CARBOXYLIC ACIDS
Manoj Kumar,1,2 Shikha Gandhi,1 Swinderjeet Singh Kalra,2 and Vinod K. Singh1
1Department of Chemistry, Indian Institute of Technology, Kanpur, India
2Department of Chemistry, D. A. V. College, Kanpur, India
Abstract
Synth. Commun. 2008, 38, 1533
FACILE SYNTHESIS OF MILL MOTH'S SEX PHEROMONE COMPONENTS
Gábor Hornyánszky, János Rohály, and Lajos Novák
Department of Organic Chemistry and Technology and Research Group for Alkaloid Chemistry of the Hungarian Academy of Sciences, University of Technology and Economics, Budapest, Hungary
Abstract
Synth. Commun. 2008, 38, 1541
SYNTHETIC STUDIES TOWARD C3‐C9 SEGMENT OF SORAPHEN A1α
Ahmad Farouk Eweas
Medicinal Chemistry Department, National Research Center, Dokki, Cairo, Egypt
Abstract
Synth. Commun. 2008, 38, 1553
SIMPLE SYNTHESIS OF DEUTERATED PTEROSINES
Gaetano Miele,1 Roberta Costi,1 Francesco Bonadies,2 and Rosario Nicoletti2
1Department of Pharmaceutical Studies, “Sapienza” University of Rome, Rome, Italy
2Department of Chemistry “Sapienza” University of Rome, Rome, Italy
Abstract
Synth. Commun. 2008, 38, 1560
NOVEL STEREOSELECTIVE SYNTHESIS OF DENSELY FUNCTIONALIZED 2H‐INDENO[2,1‐B]FURANS
Nader Noshiranzadeh,1 Ali Ramazani,1 Katarzyna Ślepokura,2 and Tadeusz Lis2
1Department of Chemistry, University of Zanjan, Zanjan, Iran
2Faculty of Chemistry, University of Wrocław, Wrocław, Poland
Abstract
Synth. Commun. 2008, 38, 1569
SIMPLE AND CONVENIENT SYNTHESIS OF 4‐UNSUBSTITUTED‐3‐(3‐OXOALKYL) ISOCOUMARINS
Alexander V. Butin,1 Artem S. Dmitriev,1 Maxim G. Uchuskin1 Vladimir T. Abaev,2 and Igor V. Trushkov3
1Research Institute of Heterocyclic Compounds Chemistry, Kuban State University of Technology, Krasnodar, Russian Federation
2Department of Chemistry, North‐Ossetian State University, Russian Federation
3Department of Chemistry, M. V. Lomonosov Moscow State University, Russian Federation
Abstract
Synth. Commun. 2008, 38, 1579
A CONVENIENT APPROACH TO THE SYNTHESIS OF DIALKYL 5‐OXO‐1,2‐DIHYDRO‐5H‐CHROMENO [4,3‐B]PYRIDINE‐2,3‐DICARBOXYLATES
Toma N. Glasnov and Ivo C. Ivanov
Faculty of Pharmacy, Department of Organic Chemistry, Medical University of Sofia, Sofia, Bulgaria
Abstract
Synth. Commun. 2008, 38, 1589
SYNTHESIS OF A NEW DITOPIC LIGAND POSSESSING LINEAR AND CYCLIC TETRAAZA SUBUNITS
Anton Prokhorov, Hélène Bernard, Nathalie Le Bris, Nicolas Marquet, and Henri Handel
Department of Chemistry, University of Brest, Brest, France
Abstract
Synth. Commun. 2008, 38, 1601
CATALYTIC TRANSFER HYDROGENATION AND HYDROGENOLYSIS IN IONIC LIQUIDS WITH Pd/MgLa MIXED OXIDE AND Pd/MgAl HYDROTALCITE AS RECYCLABLE CATALYSTS
Zoltán Baán,1 Attila Potor,1 Agnieszka Cwik,1 Zoltán Hell,1 György Keglevich,2 Zoltán Finta,2 and István Hermecz2
1Department of Organic Chemical Technology, Budapest University of Technology and Economics, Budapest, Hungary
2Chinoin Pharmaceutical and Chemical Works Ltd., Budapest, Hungary
Abstract
Synth. Commun. 2008, 38, 1610
[α‐PW12O40]3− IMMOBILIZED ON IONIC LIQUID–MODIFIED POLYMER AS A HETEROGENEOUS CATALYST FOR ALCOHOL OXIDATION WITH HYDROGEN PEROXIDE
Xianjun Lang,1,2 Zhen Li,1 and Chungu Xia1
1State Key Laboratory for Oxo Synthesis and Selective Oxidation, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou, China
2Graduate University of Chinese Academy of Sciences, Beijing, China
Abstract
Synth. Commun. 2008, 38, 1617
FeCl3‐CATALYZED NUCLEOPHILIC SUBSTITUTION OF BAYLIS–HILLMAN ADDUCTS WITH ALCOHOLS
Xueshun Jia, Peichao Zhao, Xiaotao Liu, and Jian Li
Department of Chemistry, Shanghai University, Shanghai, China
FeCl3‐catalyzed nucleophilic substitution reaction of Baylis–Hillman adducts with alcohols is described. The present protocol allows for the efficient syntheses of many kinds of functional ethers. This conversion is also a green route because water is the only side product.
Abstract
Synth. Commun. 2008, 38, 1629
DIRECT OXIDATION OF N‐BENZYLAMIDES TO ALDEHYDES OR KETONES BY N‐BROMOSUCCINIMIDE
Guangjun Wang,1,2 Zhengwei Li,3 Chengyong Ha,1 and Ke Ding3
1Key Laboratory of Cellulose and Lignocellulosics Chemistry, Guangzhou Institute of Chemistry, Chinese Academy of Sciences, Guangzhou, Guangdong, China
2Graduate School of the Chinese Academy of Sciences, Beijing, China
3Guangzhou Institute of Biomedicine and Health, Chinese Academy of Sciences, Guangzhou, Guangdong, China
Abstract
Synth. Commun. 2008, 38, 1638
HIGHLY EFFICIENT HETEROBIMETALLIC IRON‐MAGNESIUM‐HMPA–CATALYZED MICHAEL‐TYPE FRIEDEL–CRAFTS REACTIONS OF INDOLES AND CHALCONES
Wei Zhou,1,2 Li Li,2 Li‐Wen Xu1,2 Hua‐Yu Qiu,2 Guo‐Qiao Lai,2 Chun‐Gu Xia,1 and Anne‐Sophie Castanet3
1State Key Laboratory for Oxo Synthesis and Selective Oxidation, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, and Graduate School of the Chinese Academy of Sciences, Lanzhou, China
2Key Laboratory of Organosilicon Chemistry and Material Technology of Ministry of Education, Hangzhou Normal University, Hangzhou, China
3Department of Organic Molecular Macromolecular Chemistry, Faculty of Science, University of Main and CNRS, Le Mans, France
A simple bimetallic complex (Fe‐Mg‐HMPA), catalyst with dual activation was found to be an effective and promising catayst for the Michael‐type Friedel–Crafts reactions of indoles with chalcones. This novel catalytic system has the advantages of highly efficient, mild reaction conditions and exhibits high reactivity and selectivity, which make it a useful and attractive process for the synthesis of indole derivatives.
Abstract
Synth. Commun. 2008, 38, 1646
MILD AND EFFICIENT DEOXYGENATION OF AMINE‐N‐OXIDES WITH MoCl5/NaI SYSTEM
Byung Woo Yoo and Min Chol Park
Department of Advanced Materials Chemistry, Korea University, Jochiwon, Chungnam, South Korea
Abstract
Synth. Commun. 2008, 38, 1651
NEW METHOD FOR THE REDUCTION OF BENZOPHENONES WITH RANEY Ni‐Al ALLOY IN WATER
Guo‐Bin Liu,1 Hong‐Yun Zhao,1 Jia‐Da Zhu,1 Hong‐Jie He,1 and Hong‐Jie Yang,1 Thies Thiemann,2 Hideki Tashiro,3 and Masashi Tashiro4
1Department of Chemistry, Fudan University, Shanghai, China
2Interdisciplinary Graduate School of Engineering Sciences, Kyushu University, Fukuoka, Japan
3Department of Bioscience Development, School of Bioresources, Hiroshima Prefectural University, Hiroshima, Japan
4National Institute of Advanced Industrial Science and Technology Central, Tsukuba, Ibaraki Japan
Abstract
Synth. Commun. 2008, 38, 1662
THREE‐COMPONENT, ONE‐POT SYNTHESIS OF PYRAZOLO[3,4‐B] PYRIDINE DERIVATIVES IN AQUEOUS MEDIA
Da‐Qing Shi,1,2 Hao Yao,2 and Jing‐Wen Shi2
1College of Chemistry and Chemical Engineering, Key Laboratory of Organic Synthesis of Jiangsu Province, Suzhou University, Suzhou, China
2Department of Chemistry, Xuzhou Normal University, Xuzhou, China
6‐Amino‐4‐aryl‐5‐cyanopyrazolo[3,4‐b]pyridines were synthesized by a three‐component reaction of aromatic aldehydes, malononitrile, and 5‐amino‐3‐methyl‐1‐phenylpyrazole using sodium 1‐dodecanesulfonic (SDS) as catalyst in aqueous media. The reaction has the advantages of good yield, less pollution, ease of separation, and environmental friendliness.
