Combination of AlCl₃, Ionic Liquid, and Microwaves: An Efficient Method for Dehydration and 1,3-Dipolar Cycloaddition: An Unusual Observation in the Presence of Acrylonitrile

Radhika S. Kusurkar Department of Chemistry, University of Pune, Pune, IndiaCorrespondence[email protected]

Nilesh H. Naik Department of Chemistry, University of Pune, Pune, India

Prajakta N. Naik Department of Chemistry, University of Pune, Pune, India

Abstract

Use of a combination of ionic liquids in the presence of aluminium chloride and microwave irradiation was shown to be a very efficient and high-yielding method for the dehydration of aldoximes and also for 1,3-dipolar cycloadditions. Surprisingly, the presence of acrylonitrile rendered an unusual formation of substituted amide.

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ACKNOWLEDGMENTS

We are grateful to A. P. Gadgil and J. P. Chaudhari for providing IR and NMR spectra, respectively.

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Combination of AlCl₃, Ionic Liquid, and Microwaves: An Efficient Method for Dehydration and 1,3-Dipolar Cycloaddition: An Unusual Observation in the Presence of Acrylonitrile

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Combination of AlCl3, Ionic Liquid, and Microwaves: An Efficient Method for Dehydration and 1,3-Dipolar Cycloaddition: An Unusual Observation in the Presence of Acrylonitrile

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Combination of AlCl₃, Ionic Liquid, and Microwaves: An Efficient Method for Dehydration and 1,3-Dipolar Cycloaddition: An Unusual Observation in the Presence of Acrylonitrile