One-Step Synthesis and Isolation of N-(tert-Butoxycarbonyl)-N′-methylthiourea on a Large Scale

Teresa Andreani Schering-Plough Research Institute, Kenilworth, New Jersey, USA

Yan Jin Schering-Plough Research Institute, Kenilworth, New Jersey, USA

Jianshe Kong Schering-Plough Research Institute, Kenilworth, New Jersey, USA

Xian Liang Schering-Plough Research Institute, Kenilworth, New Jersey, USA

Tao Meng Schering-Plough Research Institute, Kenilworth, New Jersey, USA

Jesse K. Wong Schering-Plough Research Institute, Kenilworth, New Jersey, USACorrespondence[email protected]

Abstract

Simple preparation and isolation of N-(tert-butoxycarbonyl)-N′-methylthiourea on a large scale are described.

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ACKNOWLEDGMENT

We thank Alexei Buevich, T. M. Chan, L.-K. Zhang, and Rebecca Osterman for spectroscopic analyses, Dr. McNamara for advice and support, and H. Yun for library research.

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One-Step Synthesis and Isolation of N-(tert-Butoxycarbonyl)-N′-methylthiourea on a Large Scale

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One-Step Synthesis and Isolation of N-(tert-Butoxycarbonyl)-N′-methylthiourea on a Large Scale

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ACKNOWLEDGMENT

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