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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 40, 2010 - Issue 5
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Original Articles

Easy Access to 2,5-Anhydro-1,3-O-isopropylidene-D-glucitol

Bogdan Doboszewski Department of Chemistry, Federal Rural University of Pernambuco, Recife, BrazilCorrespondence[email protected]
&
Edmilson Clarindo de Siqueira Department of Chemistry, Federal Rural University of Pernambuco, Recife, Brazil
Pages 744-748 | Received 12 Nov 2008, Published online: 04 Feb 2010
 
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Abstract

Acid-catalyzed cyclization of D-mannitol followed by isopropylidenation furnished 2,5-anhydro-1,3-O-isopropylidene-D-glucitol, conveniently isolated by dry column vacuum chromatography.

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