Efficient Solid/Liquid Phase-Transfer Catalytic Diazo Transfer Synthesis

Zsuzsa M. Jászay Research Group of Organic Chemical Technology of the Hungarian Academy of Sciences, Budapest, HungaryCorrespondence[email protected]

Truong Son Pham Department of Organic Chemistry and Technology, Budapest University of Technology and Economics, Budapest, Hungary

Katalin Gönczi Department of Organic Chemistry and Technology, Budapest University of Technology and Economics, Budapest, Hungary

Imre Petneházy Department of Organic Chemistry and Technology, Budapest University of Technology and Economics, Budapest, Hungary

László Tőke Department of Organic Chemistry and Technology, Budapest University of Technology and Economics, Budapest, Hungary

Abstract

A simple and efficient solid/liquid phase-transfer catalytic diazo transfer reaction for the synthesis of diazocarbonyl, diazophosphonyl, and diazophosphinyl compounds is reported.

Keywords:

ACKNOWLEDGMENT

Financial support by the Hungarian Scientific Research Fund (OTKA No. K60284) is gratefully acknowledged.

Notes

^aConversion is based on ¹H NMR analysis.

^bConversion is based on ³¹P NMR analysis.

^cNew compound.

^dWith p-acetamidobenzenesulfonyl azide.

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Efficient Solid/Liquid Phase-Transfer Catalytic Diazo Transfer Synthesis

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Efficient Solid/Liquid Phase-Transfer Catalytic Diazo Transfer Synthesis

Abstract

ACKNOWLEDGMENT

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