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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 41, 2011 - Issue 19
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Original Articles

Synthesis of 4-Methylene-1,3-naphthoxazines by the Reaction of Imines with Triphosgene

Pages 2952-2958 | Received 22 Apr 2010, Published online: 29 Jun 2011
 

Abstract

Reaction of 2-acetyl-1-naphthol with aliphatic amines under microwave irradiation gave the corresponding imines (Schiff bases), which were treated with triphosgene to give 4-methylene-1,3-naphthoxazines in good yields.

ACKNOWLEDGMENT

The author is thankful to Hamad Z. Alkhathlan, professor of chemistry, King Saud University, Udaipur, for valuable suggestions and guidance.

Notes

a Yields refer to isolated products.

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