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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 41, 2011 - Issue 23
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Original Articles

Synthesis and Crystal Structure of (Z)-Ethyl 5-(phenylamino)-3-(phenylimino)-3H-1,2-dithiole-4-carboxylate

Mehtab Parveen Department of Chemistry, Aligarh Muslim University, Aligarh, UP, IndiaCorrespondence[email protected]
,
Sayed H. Mehdi Department of Chemistry, Aligarh Muslim University, Aligarh, UP, India
,
Mohammad N. Siddiqui Department of Chemistry, King Fahd University of Petroleum and Minerals, Dahran, Saudi Arabai
&
Mohammed B. Fettouhi Department of Chemistry, King Fahd University of Petroleum and Minerals, Dahran, Saudi Arabai
Pages 3469-3476 | Received 06 May 2010, Published online: 04 Aug 2011
 
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Abstract

The compound (Z)-ethyl 5-(phenylamino)-3-(phenylimino)-3H-1,2-dithiole-4-carboxylate 3 has been synthesized by the reaction of ethylacetoacetate 1 and phenylisothiocyanate 2. Its structure has been established by 1H NMR, 13C NMR, infrared, mass spectra, and x-ray crystallography.

ACKNOWLEDGMENTS

We are thankful to Prof. M. Mushfiq for useful discussion and to the chairman of the Department of Chemistry for providing the necessary facilities.

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