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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 45, 2015 - Issue 4
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Original Articles

One-Pot Direct Synthesis of Weinreb Amides from Aryl and Hetero Aryl Halides Using Co2(CO)8 as an Effective CO Source Under Conventional Thermal Heating

Poongavanam BaburajanDepartment of Chemistry, Gandhigram Rural Institute (Deemed University), Gandhigram, India
&
Kuppanagounder P. ElangoDepartment of Chemistry, Gandhigram Rural Institute (Deemed University), Gandhigram, IndiaCorrespondence[email protected]
Pages 531-538 | Received 18 Jul 2014, Published online: 31 Dec 2014
 
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Abstract

A successful protocol for the synthesis of Weinreb amides directly from aryl halides via aminocarbonylation with N,O-dimethyl hydroxylamine using Co2(CO)8 as an in situ CO source has been demonstrated. The effects of various reaction parameters such as temperature, base, and CO source have also been investigated and optimized.

GRAPHICAL ABSTRACT

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Related Research Data

One-Pot Direct Synthesis of Weinreb Amides from Aryl and Hetero Aryl Halides Using Co2(CO)8 as an Effective CO Source Under Conventional Thermal Heating
Source: Taylor & Francis
Recent advances in the transition metal catalyzed carbonylation of alkynes, arenes and aryl halides using CO surrogates
Source: Royal Society of Chemistry (RSC)

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