Synthetic Communications

An International Journal for Rapid Communication of Synthetic Organic Chemistry

Volume 48, 2018 - Issue 21

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NMP-mediated chlorination of aliphatic alcohols with aryl sulfonyl chloride for the synthesis of alkyl chlorides

Dagui ZhengKey Laboratory of Applied Organic Chemistry, Higher Institutions of Jiangxi Province, Shangrao Normal University, Shangrao, PR ChinaCorrespondence[email protected]
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Liu-Liang MaoKey Laboratory of Applied Organic Chemistry, Higher Institutions of Jiangxi Province, Shangrao Normal University, Shangrao, PR ChinaView further author information

Xian-Hong ZhuKey Laboratory of Applied Organic Chemistry, Higher Institutions of Jiangxi Province, Shangrao Normal University, Shangrao, PR ChinaView further author information

An-Xi ZhouKey Laboratory of Applied Organic Chemistry, Higher Institutions of Jiangxi Province, Shangrao Normal University, Shangrao, PR China

http://orcid.org/0000-0002-2143-0988 View further author information

Abstract

NMP-mediated chlorination of aliphatic alcohols has been developed for the synthesis of alkyl chlorides. This facile, efficient and practical approach used simple and readily available aryl sulfonyl chlorides as the chlorination reagent for the construction of C–Cl bond in good to excellent yields with mild conditions and broad substrate scope.

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The research work was supported by the financial support from the Science and Technology Research Projects of the Jiangxi Provincial Education Department [Nos. GJJ161059, GJJ151062 and GJJ14716].

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NMP-mediated chlorination of aliphatic alcohols with aryl sulfonyl chloride for the synthesis of alkyl chlorides

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NMP-mediated chlorination of aliphatic alcohols with aryl sulfonyl chloride for the synthesis of alkyl chlorides

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