Synthetic Communications

An International Journal for Rapid Communication of Synthetic Organic Chemistry

Volume 49, 2019 - Issue 20

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Total synthesis of pandangolide 1 proposed structure^*

Chada Raji ReddyDepartment of Organic Synthesis and Process Chemistry, CSIR-Indian Institute of Chemical Technology, Hyderabad, India; ;Academy of Scientific and Innovative Research (AcSIR), Ghaziabad, IndiaCorrespondence[email protected]
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Kathe MalleshDepartment of Organic Synthesis and Process Chemistry, CSIR-Indian Institute of Chemical Technology, Hyderabad, India; ;Academy of Scientific and Innovative Research (AcSIR), Ghaziabad, IndiaView further author information

Dharmapuri GajulaDepartment of Organic Synthesis and Process Chemistry, CSIR-Indian Institute of Chemical Technology, Hyderabad, India; View further author information

Uredi DilipkumarDepartment of Organic Synthesis and Process Chemistry, CSIR-Indian Institute of Chemical Technology, Hyderabad, India; View further author information

Abstract

A synthetic strategy for the proposed structure of the pandangolide 1 is disclosed starting from 1,3-propane diol in 18-steps. Sharpless asymmetric dihydroxylation, Keck allylation, Yamaguchi esterification, and Grubbs ring closing metathesis were the key steps in the synthesis.

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CRR is grateful to Council of Scientific and Industrial Research (CSIR), New Delhi for financial support as part Fast-Track Translational (FTT) project (MLP 0026).

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Total synthesis of pandangolide 1 proposed structure^*

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Total synthesis of pandangolide 1 proposed structure*

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Total synthesis of pandangolide 1 proposed structure^*