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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 49, 2019 - Issue 24
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Synthetic Communications Reviews

A convenient synthesis and crystal structure of disubstituted 1,2,3-triazoles having ether functionality

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Pages 3435-3441 | Received 26 May 2019, Published online: 14 Oct 2019
 

Abstract

A series of 27 ether-linked 1,4-disubstituted 1,2,3-triazoles (8a–8z1) has been synthesized by 1,3 dipolar cycloaddition of 1-substituted-4-(prop-2-yn-1-yloxy)benzene (3a–3c) and aromatic azides (5a–5c, 7a–7f). The synthesized compounds were explicated by FTIR, 1H NMR, 13C NMR and HRMS techniques. The structures of synthesized triazoles 8c (CCDC 1840219) and 8f (CCDC 1840220) were also confirmed by X-ray crystallography.

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Disclosure statement

No potential conflict of interest was reported by the authors.

Additional information

Funding

Authors are highly thankful to DST, New Delhi for financial assistance sanctioned to GJU S&T, Hisar under PURSE program No. SR/PURSE Phase 2/40(G) and Central Instrumentation Laboratory, GJU S&T, Hisar.

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