Synthetic Communications

An International Journal for Rapid Communication of Synthetic Organic Chemistry

Volume 51, 2021 - Issue 1

239

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Articles

Rh(III)−catalyzed synthesis of isoquinolines from N-hydroxyoximes and alkynes in γ-valerolactone

Kuan-Chang Jianga School of Petrochemical Engineering, Jiangsu Key Laboratory of Advanced Catalytic Materials and Technology, Changzhou University, Changzhou, ChinaView further author information

Liang Wanga School of Petrochemical Engineering, Jiangsu Key Laboratory of Advanced Catalytic Materials and Technology, Changzhou University, Changzhou, China;b School of Chemical and Pharmaceutical Engineering, Changzhou Vocational Institute of Engineering, Changzhou, ChinaCorrespondence[email protected]
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Qun Chena School of Petrochemical Engineering, Jiangsu Key Laboratory of Advanced Catalytic Materials and Technology, Changzhou University, Changzhou, ChinaView further author information

Ming-Yang Hea School of Petrochemical Engineering, Jiangsu Key Laboratory of Advanced Catalytic Materials and Technology, Changzhou University, Changzhou, ChinaView further author information

Ming-Gui Shenc National Engineering Laboratory for Biomass Chemical Utilization, Key and Open Laboratory on Forest Chemical Engineering, Key Laboratory of Biomass Energy and Material, Institute of Chemical Industry of Forest Products, Nanjing, ChinaView further author information

Zhi-Hui Zhanga School of Petrochemical Engineering, Jiangsu Key Laboratory of Advanced Catalytic Materials and Technology, Changzhou University, Changzhou, ChinaCorrespondence[email protected]
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Abstract

A Rh (III)−catalyzed synthesis of isoquinoline derivatives from N-hydroxyoximes and alkynes via C–H activation/annulation process in biomass-derived γ-valerolactone (GVL) has been developed. A series of functional groups were well tolerated, affording the desired products in good to excellent yields.

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We gratefully acknowledge the China Postdoctoral Science Foundation [2018M632289], the Jiangsu Key Laboratory of Advanced Catalytic Materials and Technology [BM2012110], the Priority Academic Program Development (PAPD) of Jiangsu Higher Education Institutions, and Jiangsu Key Laboratory of Biomass Energy and Material [JSBEM201806] for the financial support.

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Rh(III)−catalyzed synthesis of isoquinolines from N-hydroxyoximes and alkynes in γ-valerolactone

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Rh(III)−catalyzed synthesis of isoquinolines from N-hydroxyoximes and alkynes in γ-valerolactone

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