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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 52, 2022 - Issue 5
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Articles

Synthesis of 5-arylidene-3-(pyridin-4-yl)-2-thio-imidazolidinone derivatives with the end of flexible chain modified with aryl groups under microwave

Chongyang Maoa Institute of Biomedical Materials Industry Technology, Hubei Co-Innovation Center for Utilization of Biomass Waste, College of Chemistry and Materials Science, Hubei Engineering University, Xiaogan, Hubei, ChinaView further author information
,
Zhen Caoa Institute of Biomedical Materials Industry Technology, Hubei Co-Innovation Center for Utilization of Biomass Waste, College of Chemistry and Materials Science, Hubei Engineering University, Xiaogan, Hubei, ChinaView further author information
,
Boqiao Fua Institute of Biomedical Materials Industry Technology, Hubei Co-Innovation Center for Utilization of Biomass Waste, College of Chemistry and Materials Science, Hubei Engineering University, Xiaogan, Hubei, ChinaCorrespondence[email protected]
ORCID Iconhttps://orcid.org/0000-0002-7022-6051View further author information
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Shengcheng Wanga Institute of Biomedical Materials Industry Technology, Hubei Co-Innovation Center for Utilization of Biomass Waste, College of Chemistry and Materials Science, Hubei Engineering University, Xiaogan, Hubei, ChinaView further author information
,
Haowei Chena Institute of Biomedical Materials Industry Technology, Hubei Co-Innovation Center for Utilization of Biomass Waste, College of Chemistry and Materials Science, Hubei Engineering University, Xiaogan, Hubei, ChinaView further author information
,
Caifen Xiaa Institute of Biomedical Materials Industry Technology, Hubei Co-Innovation Center for Utilization of Biomass Waste, College of Chemistry and Materials Science, Hubei Engineering University, Xiaogan, Hubei, ChinaView further author information
,
Xinliang Hua Institute of Biomedical Materials Industry Technology, Hubei Co-Innovation Center for Utilization of Biomass Waste, College of Chemistry and Materials Science, Hubei Engineering University, Xiaogan, Hubei, ChinaView further author information
,
Xinyuan Huangb College of Life Science and Technology, Hubei Engineering University, Xiaogan, Hubei, ChinaView further author information
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Caiqin Qina Institute of Biomedical Materials Industry Technology, Hubei Co-Innovation Center for Utilization of Biomass Waste, College of Chemistry and Materials Science, Hubei Engineering University, Xiaogan, Hubei, ChinaCorrespondence[email protected]
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Pages 694-703 | Received 01 Sep 2021, Published online: 11 Mar 2022
 
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Abstract

A series of 2-thio-imidazolidinone derivatives with aryl group modifications at the end of the five-carbon side chain were synthesized. Compared with conventional heating, the target compounds were obtained in higher yield (77–95%) and shorter reaction time under the assistance of microwave heating 100 °C over 2 h.

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Additional information

Funding

This work was supported by the Natural Science Foundation of Hubei Province, China (2014CFB570).

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Synthesis of 5-arylidene-3-(pyridin-4-yl)-2-thio-imidazolidinone derivatives with the end of flexible chain modified with aryl groups under microwave
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