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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 41, 2011 - Issue 6
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Original Articles

Hexaalkoxytriphenylenes Synthesized from Facile Solvent-Free Oxidative Coupling Trimerization

Weibin Bai College of Chemistry and Material Science, Fujian Normal University, Fuzhou, China; Key Laboratory of Polymer Materials, Fuzhou, ChinaCorrespondence[email protected]
&
Jinhuo Lin College of Chemistry and Material Science, Fujian Normal University, Fuzhou, China; Key Laboratory of Polymer Materials, Fuzhou, China
Pages 903-906 | Received 26 Sep 2009, Published online: 25 Feb 2011
 
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Abstract

By grinding 1,2-dialkoxybenzene with anhydrous FeCl3 powder using a glass pestle in a mortar at ambient temperature under solvent-free conditions, hexaalkoxytriphenylenes were obtained in good yield (up to 90%) in 30 min. The solvent-free oxidative coupling reaction is a facile, efficient, “green-chemistry” method.

ACKNOWLEDGMENT

This work was supported by the Science Foundation for Youths of Fujian Province (2010J05108).

Notes

a Molecular ratio of 1,2-dialkoxybenzenes and FeCl3.

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