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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 2, 1972 - Issue 2
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Original Articles

Synteesis of 2-Adamantane Carboxylic Acid

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Pages 79-81 | Received 13 Oct 1971, Published online: 26 Jan 2007
 

Abstract

Despite the fact that there are two well-described routes to 2-adamantane carboxylic acid (IV)1,2 it is not an easily accessible compound. In connection with our work in the field of adamantane ketenes and other 2-substituted adamantane derivatives5,6 on adamantanone (I), followed by conversion of the enol ether (II) to the aldehyde (III) and oxidation of the latter to give 2-adanabtabe carvixtkuc acud (IV). The yield of this one-pot procedure is 70%-75% (about 10 runs).

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