A Convenient Synthesis of 3-Butyn-1-OL and 2-Methyl-3-Butyn-1-OL

F. Gérard Laboratoire de Chimie des Organométalliques, Groupe de Recherches de Chimie Organique, Université de Poitiers, 86022, POITIERS, CEDEX, France

Ph. Miginiac Laboratoire de Chimie des Organométalliques, Groupe de Recherches de Chimie Organique, Université de Poitiers, 86022, POITIERS, CEDEX, France

Abstract

The method reported in literature for the synthesis of 3-butyn-1-ol involves the reaction of sodium^1–7 or lithium⁸ acetylide with ethylene oxide. It needs liquid ammonia, dry ice and a rather long contact time. Moreover, yield is not consistent: 15–45%⁹.

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A Convenient Synthesis of 3-Butyn-1-OL and 2-Methyl-3-Butyn-1-OL

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A Convenient Synthesis of 3-Butyn-1-OL and 2-Methyl-3-Butyn-1-OL

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