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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 12, 1982 - Issue 6
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Original Articles

Two Novel Syntheses of Substituted 1,2,4-Oxadiazoles from Amidoximes

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Pages 457-461 | Published online: 05 Dec 2006
 

Abstract

The classical preparation of 1,2,4-oxadiazoles through the reaction of amidoximes with acylating agents such as acyl chlorides or anhydrides has been described frequently1–3. The synthesis proceeds via the O-acylamidoximes which are, however, not often isolated. Instead of acyl chlorides or anhydrides, other reagents have been used, such as ketene, mixed anhydrides, carboxylic azides and thioacetic acid1.

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