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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 13, 1983 - Issue 10
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Original Articles

A Simple Regiospecific Synthesis of Monodeuterioalkenes from Non-Deuterated Precursors via the Wittig Reaction Using Deuterated Solvents and Bases

David Beeman Department of Chemical Engineering & Chemistry, New Jersey Institute of Technology, Newark, New Jersey, 07102, USA
,
Charles Wenger Department of Chemical Engineering & Chemistry, New Jersey Institute of Technology, Newark, New Jersey, 07102, USA
&
Howard D. Perlmutter Department of Chemical Engineering & Chemistry, New Jersey Institute of Technology, Newark, New Jersey, 07102, USA
Pages 853-861 | Published online: 05 Dec 2006
 
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Abstract

The use of deuterated water and alcohols and bases derived from them allows one to prepare monodeuterated alkenes by the Wittig reaction of non-deuterated phosphonium salts and aldehydes and ketones.

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