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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 14, 1984 - Issue 6
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Original Articles

Mannich Reaction Under High Pressee. Dimethylaminomethylation of Ketones with bis(Diyethylamino)methane under Mild Conditions

Kiyoshi Matsumoto College of liberal Arts & Sciences, Kyoto University, Kyoto, 606, Japan
,
Shiro Hashimoto College of liberal Arts & Sciences, Kyoto University, Kyoto, 606, Japan
,
Shinichi Otani College of liberal Arts & Sciences, Kyoto University, Kyoto, 606, Japan
,
Fujitsugu Atnita Department of Chemistry, Faculty of Science, Kyoto University, Kyoto, 606, Japan
&
Jiro Osugi Department of Chemistry, Faculty of Science, Kyoto University, Kyoto, 606, Japan; College of liberal Arts & Sciences, Kyoto University, Kyoto, 606, Japan
Pages 585-590 | Published online: 06 Dec 2006
 
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Abstract

Dimethylaminomethylation of ketones with bis(dimethyl-amino)methane takes place cleanly in methanol at room temperature in the kiro bar region.

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