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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 14, 1984 - Issue 11
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Original Articles

Fluoroaconitates: Wittig Reaction of Oxalofluoroacetic Acid Esters

D. Cantacuzéne C.N.R.S.-C.E.R.C.O.A., 2, rue Henri Dunant, 94320, Thiais, France
,
C. Wakselman C.N.R.S.-C.E.R.C.O.A., 2, rue Henri Dunant, 94320, Thiais, France
&
H. Massoudi C.N.R.S.-C.E.R.C.O.A., 2, rue Henri Dunant, 94320, Thiais, France
Pages 1067-1072 | Published online: 06 Dec 2006
 
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Abstract

Triphenylcarboalcoxymethylene phosphoranes 1 are condensed with oxalofluoroacetic acid diesters 2. Allylic fluoroaconitates 3 and their vinylic isomers 4 are Obtained. The amount of 4 decreases if lithium bromide is added to the reaction mixture.

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