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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 14, 1984 - Issue 3
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Original Articles

Decomposition of S-Alkylisothiouronium Salts Under Anhydrous Conditions - Application to a Facile Preparation of Nonsymmetrical Dialkyl Sulfides

Frederick A. Luzzio Product Technology Division, Arthur D. Little, Inc., Cambridge, Massachusetts, 02140; Department of Chemistry, Harvard University, Cambridge, Massachusetts, 02138
Pages 209-214 | Published online: 05 Dec 2006
 
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Abstract

S-Alkylisothiouronium salts are decomposed with sodium ethoxide/ethanol or sodium hydride/tetrahydrofuran to the salt of the corresponding thiols which are trapped by various electrophiles to yield nonsymmetrical dialkyl sulfides.

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