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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 14, 1984 - Issue 1
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Original Articles

A Simple and Efficient Synthesis of Ethyl and Methyl Glyoxylate

James M. Hook University Chemical Laboratories, Lensfield Road, Cambridge, CB2 1EW, England; Department of Organic Chemistry, University of New South Wales, Kensington, NSW, Australia, 2033
Pages 83-87 | Published online: 05 Dec 2006
 
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Abstract

Ethyl and methyl glyoxylate are both prepared in high yields from an exchange reaction between the appropriate alkyl dialkoxyacetate and glyoxylic acid, followed by reaction with phosphorus pentoxide.

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