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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 15, 1985 - Issue 7
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Original Articles

Reactions of Nitrile Oxides With Phenylsulphinylpropa-1,2, Diene and 1-Phenylthioprop-2-ENE. New Routes to Functionalised α,β-Unsaturated Ketone Equivalents

Roger S. Brown Department of Chemistry, The University, Southampton, S09 5NH, U.K.
,
Philip J. Parsons Department of Chemistry, The University, Southampton, S09 5NH, U.K.
&
Stephen C. Eyley Fisons plc, Pharmaceutical Division, S & T Laboratories, Bakewell Road, Loughborough, Leicestershire LEll OQY, U.K.
Pages 633-642 | Published online: 05 Dec 2006
 
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Abstract

Nitrile oxides add regiospecifically to the terminal double bonds in (1) and (3). The adducts (4a-e) were readily cleaved and converted into enone equivalents (8).

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