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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 15, 1985 - Issue 10
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Original Articles

Thermolysis of the Chlorofluorocarbene 1-Ethoxy-1-Phenoxyethylene Adduct to Phenyl 2-Fluoroacrylate

T. Nguyen C.N.R.S.-C.E.R.C.O.A., 2 à 8, rue Henri, Dunant, 94320, Thiais, (France)
,
H. Molines C.N.R.S.-C.E.R.C.O.A., 2 à 8, rue Henri, Dunant, 94320, Thiais, (France)
&
C. Wakselman C.N.R.S.-C.E.R.C.O.A., 2 à 8, rue Henri, Dunant, 94320, Thiais, (France)
Pages 925-930 | Published online: 05 Dec 2006
 
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Abstract

The preparation of 1-ethoxy-1-phenoxyethylene 1 is described. Its condensation with chlorofluorocarbene gives 2,2-chlorofluorocyclopropanone acetal 2, thermolysis of which leads to phenyl 2-fluoroacrylate 3.

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