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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 15, 1985 - Issue 13
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Original Articles

An Efficient Route to 2-(Formylmethyl)-Cyclopenten-3-one and Its 1-methyl-Congener

David A. Armstead Department of Chemistry, University of Reading, Whiteknights, P.O. Box 224, Reading, Berkshire, RG6 2AD, U.K.
&
John Mann Department of Chemistry, University of Reading, Whiteknights, P.O. Box 224, Reading, Berkshire, RG6 2AD, U.K.
Pages 1147-1151 | Published online: 19 Dec 2006
 
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Abstract

We describe a five-step synthesis of 2-(formylmethyl) - cyclopenten-3-one (1a) and its 1-methyl congener (1b) from 6-methylhept-5-ene-2-one by way of the respective 2-(3-methylbut-2-enyl)-cyclopenten-3-ones (5) and selective ozonolysis of these intermediates.

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