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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 17, 1987 - Issue 15
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Original Articles

Electrooxidative Cleavage of Carbon-Carbon Bonds. III. Preparation of Alkanediones from Cycloalkanones Through 2-Phenylthio-1-Cycloalkanols

Sigeru Torii Department of Industrial Chemistry, School of Engineering, Okayama University, Tsushima, Okayama, Japan, 700
,
Tsutomu Inokuchi Department of Industrial Chemistry, School of Engineering, Okayama University, Tsushima, Okayama, Japan, 700
&
Yoshihiro Araki Department of Industrial Chemistry, School of Engineering, Okayama University, Tsushima, Okayama, Japan, 700
Pages 1797-1805 | Published online: 19 Dec 2006
 
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Abstract

The tittle electrochemical procedures have been carried out either in a divided cell, giving keto acetals 3 from 2 (R1 = H, R2 = alkyl), or in an undivided cell, affording diketones 4 from 2 (R1 = R2 = alkyl), in moderate to good yields.

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